鼠曲草TLC鉴别及质量检查项目研究 |
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引用本文: | 张立庆,曲畅游,李渤文,肖海燕,路立峰. 鼠曲草TLC鉴别及质量检查项目研究[J]. 山东医药工业, 2014, 0(9): 511-513 |
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作者姓名: | 张立庆 曲畅游 李渤文 肖海燕 路立峰 |
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作者单位: | 山东药品食品职业学院,山东威海264210 |
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基金项目: | 山东省食品药品监督管理局2011年立项项目--《山东省中药材标准》、《山东省中药饮片炮制规范》(2012年版)标准研究 |
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摘 要: | 目的建立简单快捷的鼠曲草药材质量控制方法和标准。方法通过对3个不同产地的鼠曲草药材进行TLC鉴别、水溶性浸出物、醇溶性浸出物、水分以及灰分测定的研究,建立其质量控制标准。结果确定了鼠曲草TLC鉴别、水分、灰分和水溶性浸出物、醇溶性浸出物的测定方法,制定了其质量控制标准。结论研究结果表明本研究制定的鼠曲草药材质量控制标准,可为山东省以及其他地区使用和检验提供依据。
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关 键 词: | 鼠曲草 薄层色谱鉴别 水分检查 灰分检查 水溶性浸出物 醇溶性浸出物 |
Study on TLC identification and quality inspection project of Gnaphalium affine |
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Affiliation: | ZHANG Li-qing, QU Chang-you, LI Bo-wen,XIAO Hai-yan, L U Li-feng ( Shandong Drug and Food Vocational College, Weihai 264210, China ) |
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Abstract: | Objective To establish a simple and rapid quality control method and standard for Gnaphalium affine quantification. Methods Samples from three different regions were studied on TLC identification. The moisture, ashes, wa- ter - soluble and ethanol - soluble extractives of these samples were determined to establish the quality control standard. Re- sults Quality control standard was developed by the confirmed indicators : TLC identification, moisture, ash, water - soluble extract and alcohol - soluble extract of Gnaphalium affine. Conclusion The quality control standard for the Gnaphalium af- fine established by this research could provide the testing basis for Shandong Province and other regions. |
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Keywords: | Gnaphalium affine TLC identification Moisture test Ashes test Water - soluble extractive Ethanol - solu-ble extractive |
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