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| 心痛宁片质量标准研究 | |
| 引用本文： | 罗艳萍,陈建,黄礼杰,甄汉深. 心痛宁片质量标准研究[J]. 中成药, 2007, 29(2): 224-227 |
| 作者姓名： | 罗艳萍 陈建 黄礼杰 甄汉深 |
| 作者单位： | 1. 浙江佐力药业股份有限公司,浙江,湖州,313200 2. 深圳药源医药科技开发公司,广东,深圳,518057 3. 广西中医学院药学院,广西,南宁,530021 |
| 摘 要： | 目的:建立心痛宁片(人参、丹参等)的质量标准。方法:采用薄层色谱法鉴别心痛宁片中丹参、姜黄、熊胆粉;高效液相色谱法对制剂中的人参皂苷Rg1、Re进行定量分析。结果:薄层色谱法均能对丹参、姜黄、熊胆粉进行专属性定性分析;含量测定人参皂苷Rg1平均回收率97.18%,人参皂苷Re平均回收率96.74%(n=5)。结论:所建立的方法可准确地进行定性和定量检测,方法可靠、重复性好,可有效控制心痛宁片的质量。 |
| 关 键 词： | 心痛宁片 质量标准 人参皂苷Rg1、Re |
| 文章编号： | 1001-1528（2007）02-0224-04 |
| 修稿时间： | 2006-01-05 |
Quality standard for Xintongning Tablets |
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| LUO Yan-ping,CHEN Jian,HUANG Li-jie,ZHEN Han-shen. Quality standard for Xintongning Tablets[J]. Chinese Traditional Patent Medicine, 2007, 29(2): 224-227 | |
| Authors: | LUO Yan-ping CHEN Jian HUANG Li-jie ZHEN Han-shen |
| Affiliation: | 1. Zhejiang Jolly Pharmaceutical Co. , Ltd. , Huzhou 313200, China; 2. Shen.zhen Yaoyaun Med-science Development Company, Shenzhen 518057, China; 3. Pharmaceutical School, Gnangxi College of TCM , Nanning 530021, China |
| Abstract: | AIM: To establish the quality sdandard for Xintongning Tablet(Radix et Rhizoma Ginseng,Radix et Rhizoma Salviae Miltiorrhizae,etc.) METHODS: TLC was used to indentify Radix et Rhizoma Salviae miltiorrhizae,Rhizoma Curcumae Longae and Fel Ursi Powder.The contents of ginsenoside Rg_1,Re were determined by HPLC. RESULTS: Radix et Rhizema Salviae miltiorrhizae,Rhizoma Curcumae Longa and Fel Ursi Powder could be indentified by TLC.The average recoveries of ginsenside Rg_1,Re were 97.18% and 96.74% respectively(n=5). CONCLUSION: The methods are reliable and reproducible.It can be used for quality control of Xintongning Tablets. |
| Keywords: | HPLC TLC |
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