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| 补骨脂炮制工艺的超高效液相色谱指纹图谱法优化 | |
| 引用本文： | 杨荣平,秦伟瀚,林芳,王云红. 补骨脂炮制工艺的超高效液相色谱指纹图谱法优化[J]. 时珍国医国药, 2012, 23(3): 699-701 |
| 作者姓名： | 杨荣平 秦伟瀚 林芳 王云红 |
| 作者单位： | 1. 重庆市中药研究院,重庆400065;中国科学院大连化学物理研究所,辽宁大连116023 2. 重庆市中药研究院,重庆,400065 3. 成都中医药大学,四川成都,610075 |
| 基金项目： | 国家自然科学基金青年基金 |
| 摘 要： | 目的优选补骨脂炮制的最佳工艺。方法从炮制方法、加盐量、加水量、浸润时间、炮制温度、炮制时间6个因素进行考察,采用超高效液相色谱(UPLC)指纹图谱法优化补骨脂炮制工艺。结果补骨脂的最佳炮制工艺是:每100 g药材,加入15 ml含盐量为2.5 g的盐溶液,浸润5 h后,置锅内,260℃加热,炒2～3 min。结论采用UPLC指纹图谱法优化补骨脂炮制工艺是合理可行。 |
| 关 键 词： | UPLC指纹图谱法 补骨脂 炮制工艺 |
The Optimization for the Processing Technology of Psoralea corylifolia L.by UPLC Fingerprint |
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| YANG Rong-ping , QIN Wei-han , LIN Fang , WANG Yun-hong. The Optimization for the Processing Technology of Psoralea corylifolia L.by UPLC Fingerprint[J]. Lishizhen Medicine and Materia Medica Research, 2012, 23(3): 699-701 | |
| Authors: | YANG Rong-ping QIN Wei-han LIN Fang WANG Yun-hong |
| Affiliation: | 1.Chongqing Academy of Chinese Materia Medica,Chongqing 400065,China;2.Dalian Institute of Chemical Physics,Chinese Academy of Sciences,Dalian 116023,China;3.Chengdu University of Traditional Chinese Medicine,Chengdu,Sichuan 610075,China) |
| Abstract: | Objective To optimize the best processing technology of Psoralea corylifolia L. Methods The processing method,the amount of added salt,added water,time for soaking,temperature and time for roasting were choosen as investigated factors.UPLC fingerprint was adopted to select the best processing methods. Results The best processing technology was set as follows: adding 15ml water containing 2.5 g salt per 100 g of psoralea corylifolial,soaking for 5 hours in the airtight container,heating at 260℃,roasting for 2~3 minutes. Conclusion Using UPLC fingerprint to optimize the processing technology of Psoralea corylifolia L.is reasonable and feasible. |
| Keywords: | UPLC fingerprint method Psoralea corylifolia L The processing technology |
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