| 清炎滴丸的质量控制 |
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| 引用本文： | 张新建,郭美华,刘志宇,哈力,庄海英,翟登奎.清炎滴丸的质量控制[J].中国药师,2014(1):46-48. |
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| 作者姓名： | 张新建 郭美华 刘志宇 哈力 庄海英 翟登奎 |
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| 作者单位： | 哈尔滨医科大学附属第一医院药学部 哈尔滨 150001;哈尔滨医科大学附属第一医院药学部 哈尔滨 150001;哈尔滨医科大学附属第一医院药学部 哈尔滨 150001;哈尔滨医科大学附属第一医院药学部 哈尔滨 150001;哈尔滨医科大学附属第一医院药学部 哈尔滨 150001;哈尔滨医科大学附属第一医院药学部 哈尔滨 150001 |
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| 基金项目： | 黑龙江省中医药科研项目(ZHY12- Z156) |
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| 摘 要： | 目的：建立清炎滴丸的质量控制标准.方法：采用薄层色谱法鉴别本品中的肿节风、苦玄参等成分;以高效液相色谱法测定本品中有效成分异嗪皮啶的含量;并建立其他相关质控指标.结果：薄层色谱斑点清晰,重复性好,专属性强.含量测定方法准确可靠,线性范围为0.042～0.839 μg,线性关系良好（R2=0.999 4）,平均回收率为98.28%（RSD=1.02%）,精密度良好.结论：建立的质量控制方法可靠、准确、全面,可用于本品的质量控制.
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| 关 键 词： | 清炎滴丸 质量控制 薄层色谱法 高效液相色谱法 异嗪皮啶 |
| 收稿时间： | 7/1/2013 12:00:00 AM |
| 修稿时间： | 2013/10/16 0:00:00 |
Study on Quality Control of Qingyan Dropping Pills |
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| Zhang Xinjian,Guo Meihu,Liu Zhiyu,Ha Li,Zhuang Haiying and Zhai Dengkui.Study on Quality Control of Qingyan Dropping Pills[J].China Pharmacist,2014(1):46-48. |
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| Authors: | Zhang Xinjian Guo Meihu Liu Zhiyu Ha Li Zhuang Haiying and Zhai Dengkui |
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| Institution: | The First Affiliated Hospital of Harbin Medical University, Harbin 150001, China;The First Affiliated Hospital of Harbin Medical University, Harbin 150001, China;The First Affiliated Hospital of Harbin Medical University, Harbin 150001, China;The First Affiliated Hospital of Harbin Medical University, Harbin 150001, China;The First Affiliated Hospital of Harbin Medical University, Harbin 150001, China;The First Affiliated Hospital of Harbin Medical University, Harbin 150001, China |
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| Abstract: | Objective： To establish the quality standard for Qingyan drol/ping pills. Methods： TLC identific, ation was used tor Sar- candraglabra （ Thunb. ） Nakai and Picria fel-terrae. The content of isofraxidin was determined by RP-HPLC. The other quality standards were established as well. Results： TI,C spols were clear with good reproducibility and specificity. The content determination method was accurate and reliable. Tile linear range of isofraxidin was 0. 042-0. 839 μg（ R2 = 0.999 4） , and the average recovery was 98.28% （ PSD = 1.02% ）. Conclusion ： The quality control method is aecurate, reliable and comprehensive, which can be used to control the quality of Qingyan dropping pills |
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| Keywords: | Qingyan dropping pills Quality standards TLC HPLC Isofraxidin |
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