| 高效液相梯度法测定红花牡丹膏中人参皂苷Rg1、Rb1、Re及三七皂苷R1的含量 |
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| 引用本文： | 黄晓其,曾宝,苏子仁.高效液相梯度法测定红花牡丹膏中人参皂苷Rg1、Rb1、Re及三七皂苷R1的含量[J].中国医院药学杂志,2007,27(10):1393-1396. |
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| 作者姓名： | 黄晓其 曾宝 苏子仁 |
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| 作者单位： | 广州中医药大学新药研究开发中心,广东,广州,510405 |
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| 摘 要： | 目的:建立红花牡丹膏中有效成分的含量测定方法。方法:采用高效液相色谱梯度法测定红花牡丹膏中有效成分含量。结果:三七中人参皂苷Rg1、Rb1、Re及三七皂苷R14种成分均达到良好分离,在测定范围内线性良好,回收率在98%~101%之间。结论:所建立的定量方法简便可行、重复性好,可用于红花牡丹膏的质量监控。
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| 关 键 词： | 高效液相色谱法 红花牡丹膏 人参皂苷Rg1 人参皂苷Rb1 人参皂苷Re 三七皂苷R1 |
| 文章编号： | 1001-5213（2007）10-1393-04 |
| 修稿时间： | 2006-08-06 |
Determination of ginsenoside Rg1,Rb1,Re and notoginsenoside R1 in Honghua Mudan ointment by HPLC |
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| HUANG Xiao-qi,ZENG Bao,SU Zi-ren.Determination of ginsenoside Rg1,Rb1,Re and notoginsenoside R1 in Honghua Mudan ointment by HPLC[J].Chinese Journal of Hospital Pharmacy,2007,27(10):1393-1396. |
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| Authors: | HUANG Xiao-qi ZENG Bao SU Zi-ren |
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| Institution: | Guangzhou University of Traditional Chinese Medicine, Guangdong Guangzhou 510405,China |
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| Abstract: | OBJECTIVE To establish a method of HPLC assay for simultaneous determining ginsenoside Rg1,Rb1,Re and notoginsenoside R1 in Honghua Mudan ointment.METHODSThe effective components in Honghua Mudan ointment were determined by HPLC.RESULTSThe resolution and the linearity were fine.The average recoveries of ginsenoside Rg1,Rb1,Re and notoginsenoside R1were 99.14%,(RSD 0.83%),99.18%,(RSD 1.26%), 99.39%,(RSD 1.24%) and 99.05%,(RSD 1.15%) separately.CONCLUSIONThe quantitative method for determinating the ingredients of Honghua Mudan ointment is simple,feasible and repeatable,and is beneficial for quality control of Yishenling Granules. |
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| Keywords: | HPLC Honghua Mudan ointment ginsenoside Rg1 ginsenoside Rb1 ginsenoside Re notoginsenoside R1 |
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