| 舒筋活血胶囊质量标准研究 |
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| 引用本文： | 吴燕.舒筋活血胶囊质量标准研究[J].青岛医药卫生,2009,41(3):206-208. |
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| 作者姓名： | 吴燕 |
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| 作者单位： | 浙江省杭州市浙江大学医学院附属邵逸夫医院药剂科,310016 |
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| 摘 要： | 目的建立舒筋活血胶囊的质量标准。方法采用薄层色谱法（TLC）对制剂中的香附、红花和香加皮进行鉴别，采用高效液相色谱法（HPLC）测定制剂中4-甲氧基水杨醛的含量。结果TLC能较好地鉴别制剂中的香附、红花和香加皮；HPLC法能准确测定出制剂中4-甲氧基水杨醛的含量，其在2-751μg／ml范围之间呈良好的线性关系，平均回收率为96．6％（RSD=0．78％）。结论所建立的方法简单可行，能快速准确地对舒筋活血胶囊进行鉴别和含量测定。
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| 关 键 词： | 舒筋活血胶囊 质量标准 薄层色谱 高效液相色谱 4-甲氧基水杨醛 |
Study on Quality Criteria of Shujin Huoxue Capsules |
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| Wu Yan.Study on Quality Criteria of Shujin Huoxue Capsules[J].QINGDAO Medical Journal,2009,41(3):206-208. |
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| Authors: | Wu Yan |
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| Institution: | Wu Yan.Shao Yifu Hospital of Medical College,Zhejiang University.Hangzhou,310016 |
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| Abstract: | Objective To establish the quality criteria of Shujin Huoxue Capsules. Methods Rhizoma Cyperi, Carthamus tinctorius and Cortex Periplocae in Shujin Huoxue Capsules were identified by thin layer chromatography（TLC）. 4-methoxysalicylal was determined by HPLC. Results The characteristic identification of Rhizoma Cyperi, Carthamus tinctorius and Cortex Periplocae by TLC was distinct and highly specific. The linear range of 4-methoxysalicylal for quantitative evaluation was 2-75μg/ml and the average recovery was 96.6%（RSD=0. 78%）. Conclusion This established method is accurate for controlling the quality of Shujin Huoxue Capsules. |
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| Keywords: | Shujin Huoxue Capsules Quality criteria TLC HPLC 4-methoxysalicylal |
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