| 香荷药条的质量标准研究 |
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| 引用本文： | 邓远辉,杨柳,丘小惠,董玉珍. 香荷药条的质量标准研究[J]. 中药材, 2001, 24(9): 672-673 |
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| 作者姓名： | 邓远辉 杨柳 丘小惠 董玉珍 |
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| 作者单位： | 广东省中医院, |
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| 摘 要： | 目的研究香荷药条的质量标准,建立黄连、苦参、丁香的薄层色谱鉴别方法和小檗碱、巴马亭的高效液相色谱含量测定方法;方法流动相为乙腈-水(11,1000ml含KH2PO43.4g,CH3(CH2)11SO4Na1.7g),检测波长345nm,样品提取过滤后进行分析;结果回归方程、相关系数及线性范围分别为小檗碱Y=1.41×105X+5.46×106,r=0.9999,线性范围0.07～2.24μg;巴马亭Y=1.96×105X+6.81×106,r=0.9997,线性范围0.07～2.24μg;结论该方法适用于香荷药条的质量控制.
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| 关 键 词： | 香荷药条 薄层色谱法 高效液相色谱法 定性鉴别 含量测定 质量标准 |
| 修稿时间： | 2001-06-28 |
Study on the Quality Standards for Xianghe Suppository |
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| Deng Yuanhui,Yang Liu,Qiu Xiaohui,Dong Yuzhen. Study on the Quality Standards for Xianghe Suppository[J]. Journal of Chinese medicinal materials, 2001, 24(9): 672-673 |
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| Authors: | Deng Yuanhui Yang Liu Qiu Xiaohui Dong Yuzhen |
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| Affiliation: | Guangdong Provincial Hospital of TCM, Guangzhou 510120. |
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| Abstract: | The quality standards for Xianghe suppository were studied. The TLC methods for identification of Rhizoma Coptidis, Radix Sophorae Flavescentis and Flos Caryophylli were established . A simple high performance liquid chromatographic method was established for de-termination of berberine and palmatine. The mobile phase was acetonitrile-water( 1:1, containing KH2PO4 3.4 g, CH3 ( CH2) 11 SO4Na 1.7 g per 1000 ml). UV detecting wavelength was 345 nm. This method is suitable for the quality control of Xianghe suppository. |
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| Keywords: | Xianghe suppository TLC HPLC |
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