| 乙酸仲丁酯的合成工艺研究 |
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| 引用本文： | 柴佳莉,周淑晶,白术杰,袁恒光. 乙酸仲丁酯的合成工艺研究[J]. 黑龙江医药科学, 2007, 30(2): 23-23 |
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| 作者姓名： | 柴佳莉 周淑晶 白术杰 袁恒光 |
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| 作者单位： | 佳木斯大学化学与药学院,黑龙江,佳木斯,154007;东北农业大学资源环境学院,黑龙江,哈尔滨,150030 |
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| 摘 要： | 目的：改进乙酸仲丁酯的合成工艺。方法：采用三氯化铁为催化剂，环已烷为带水剂，探讨了乙酸仲丁酯合成中的影响因素，应用正交设计确定最佳工艺条件。结果：在最佳试验条件下乙酸仲丁酯收率达93．8％。结论：本方法操作简便，适合工业化生产。
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| 关 键 词： | 三氯化铁 乙酸仲丁酯 正交设计 |
| 文章编号： | 1008-0104(2007)02-0023-01 |
| 修稿时间： | 2007-01-16 |
Synthesis technology of Sec-butylacetate |
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| CHAI Jia-li,ZHOU Shu-jing,BAI Shu-jie,YUAN Heng-guang. Synthesis technology of Sec-butylacetate[J]. Heilongjiang Medicine and Pharmacy, 2007, 30(2): 23-23 |
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| Authors: | CHAI Jia-li ZHOU Shu-jing BAI Shu-jie YUAN Heng-guang |
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| Abstract: | Objective:To improve the synthesis technology of Secbutylacetate.Method:We used iron chloride as the catalysis and cyclohexane as the dewatering reagent to study synthesis process of Sec-butylacetate,and established the optimal technological conditions by using orthogonal design.Result:In optimal conditions,the yield of Sec-butylacetate was over 93.8%.Conclusion:The process is simple and suitable for industrial production. |
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| Keywords: | ron chloride Sec-butylacetate orthogonal design |
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