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蒲地兰消炎片质量标准研究
引用本文:冯希勇. 蒲地兰消炎片质量标准研究[J]. 现代中药研究与实践, 2008, 22(2): 38-40
作者姓名:冯希勇
作者单位:徐州生物工程高等职业学校,江苏,徐州,221006
摘    要:目的建立蒲地兰消炎片质量标准。方法用TLC方法鉴别,RP-HPLC方法含量测定。结果TLC鉴别黄芩苷斑点清晰可辨,杂质无影响;黄芩苷线性范围为6.12-61.2μg.mL^-1,r=0.999 9;平均加样回收率为98.19%,RSD%为1.10%。结论该方法结果准确,重现性好,专属性强,可用于蒲地兰消炎片的质量控制。

关 键 词:黄芩苷  TLC  HPLC
文章编号:1673-6427(2008)01-0038-03
修稿时间:2007-09-24

Study on Quality Control Standards of Pudilan Xiaoyan Tablets
FENG Xi-yong. Study on Quality Control Standards of Pudilan Xiaoyan Tablets[J]. Research and Practice on Chinese Medicines, 2008, 22(2): 38-40
Authors:FENG Xi-yong
Affiliation:FENG Xi-yong ( Xuzhou Higher Vocational College of Bioengineered, Xuzhou 221006, China)
Abstract:Objective To establish a quality standard of Pudilan Xiaoyan tablets.Methods The principal drug-Radix Seutellariae was identified by TLC and its active ingredient of Baicalin was determined by HPLC.Results The dots of TLC was clear with a good separation degree.The linear of Baicalin was obtained in the range of 6.12~ 61.2 μg· L-1,and the average recovery was 98.19% with RSD of 1.1%.Conclusion The method was accurate and reliable with a specificity and can be used for the quality control of Pudilan Xiaoyan tablets.
Keywords:Pudilan Xiaoyan tablets  baicalin  TLC  HPLC
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