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瘀血痹胶囊质量标准研究
引用本文:金凤环.瘀血痹胶囊质量标准研究[J].中国医药导报,2008,5(18):13-15.
作者姓名:金凤环
作者单位:辽宁好护士集团本溪制药有限公司,辽宁本溪,117000
摘    要:目的:建立瘀血痹胶囊质量标准。方法:采用薄层色谱法对瘀血痹胶囊中威灵仙、当归、黄芪进行薄层定性鉴别;采用高效液相色谱法对其中的丹酚酸B进行了含量测定。结果:在薄层色谱中可检出威灵仙、当归、黄芪的特征斑点。丹酚酸B在0.2188~2.1880μg线性关系良好(r=0.9999),方法的平均回收率为100.49%(RSD=1.80%)。结论:本法操作简便、准确、重现性好,能够较好地控制瘀血痹胶囊的质量。

关 键 词:瘀血痹胶囊  薄层色谱法  高效液相色谱法  丹酚酸B

Quality standard for Yuxuebi Capsules
JIN Feng-huan.Quality standard for Yuxuebi Capsules[J].China Medical Herald,2008,5(18):13-15.
Authors:JIN Feng-huan
Institution:JIN Feng-huan (Liaoning Herbapex Group Benxi Pharmaceutical Co. LTD., Benxi 117000, China)
Abstract:Objective: To establish the quality standard of Yuxuebi Capsules. Methods: TLC identifications of Radix Et Rhizoma Clematidis ,Radix Angelicae Sinensis and Radix Astragali in Yuxuebi Capsules were carried out.The contents of salvianolic acid B were determined by means of HPLC.Results: The linear range of salvianolic acid B was 0.218 8- 2.188 0μg(r=0.999 9); the average recovery was 100.49% (RSD=1.80%). Conclusion: The methods reported in this paper are easy to operate and can provide accurate and reproducible results, thus are able to control the quality of Yuxuebi Capsules.
Keywords:Yuxuebi Capsules  TLC  HPLC  Salvianolic acid B
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