2-(1-咪唑基)乙胺的合成 |
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引用本文: | 江来恩,邓胜松,李婷婷,姚日生. 2-(1-咪唑基)乙胺的合成[J]. 中国医药工业杂志, 2010, 41(4) |
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作者姓名: | 江来恩 邓胜松 李婷婷 姚日生 |
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作者单位: | 合肥工业大学化学工程学院,安徽合肥,230009 |
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摘 要: |
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Synthesis of 2- (1-Imidazolyl) ethanamine |
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Abstract: | 2- (1-Imidazolyl) ethanamine was synthesized from ethyl acrylate by Michael addition with imidazole to give ethyl 3- (1-imidazolyl) propionate, which was subjected to hydrazinolysis, followed by the Curtius rearrangement and hydrolysis with an overall yield of about 72%. |
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Keywords: | 2-(1-imidazolyl) ethanamine intermediate synthesis |
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