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黄芩中黄芩素的提取方法考察
引用本文:高声传,王童超,肖江宁. 黄芩中黄芩素的提取方法考察[J]. 解放军药学学报, 2011, 27(6): 502-505. DOI: 10.3969/j.issn.1008-9926.2011.06.010
作者姓名:高声传  王童超  肖江宁
作者单位:沈阳军区总医院药剂科,辽宁沈阳,110016
摘    要:目的 研究纤维素酶酶解生黄芩药材的最佳酶解条件和黄芩素的最佳提取工艺.方法 采用高效液相色谱法测定黄芩素含量,以提取率为指标,分别考察浸提倍数、加酶量、pH值、温度、时间对纤维素酶酶解反应的影响,采用正交实验对乙醇浓度、提取温度、提取时间进行考察,并分别考察乙醇用量和提取次数对黄芩素提取率的影响.结果 确定了纤维素酶酶...

关 键 词:纤维素酶  黄芩素  提取率

Study on Extraction of Baicalein in Scutellaria Bacalensis
GAO Sheng-chuan,WANG Tong-chao,XIAO Jiang-ning. Study on Extraction of Baicalein in Scutellaria Bacalensis[J]. Pharmaceutical Journal of Chinese People's Liberation Army, 2011, 27(6): 502-505. DOI: 10.3969/j.issn.1008-9926.2011.06.010
Authors:GAO Sheng-chuan  WANG Tong-chao  XIAO Jiang-ning
Affiliation:GAO Sheng-chuan,WANG Tong-chao,XIAO Jiang-ning Department of Pharmacy,General Hospital of Shenyang Military Region,Shenyang 110016,China
Abstract:Objective To study the optimal cellulolysis condition of raw Scutellaria baicalensis Georgi and the optimal extraction condition of baicalein in Scutellaria bacalensis.Methods High performance liquid chromatography method was used to determine the content of baicalein in Scutellaria baicalensis.Five factors were studied on enzymatic extraction of celluase.The orthogonal experiment was adopted to study the effect of the concertration and amount of alcohol,times of refluxing,duration of refluxing and temperat...
Keywords:enzymic  baicalein  extraction rate  
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