| 川芎饮片的FTIR及其挥发油的GC-MS分析 |
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| 引用本文： | 崔丽君,张桂芝,吴海燕.川芎饮片的FTIR及其挥发油的GC-MS分析[J].亚太传统医药,2011,7(12):20-22. |
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| 作者姓名： | 崔丽君 张桂芝 吴海燕 |
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| 作者单位： | 1. 徐州师范大学化学化工学院,江苏徐州221116;徐州市中医院,江苏徐州221009
2. 徐州师范大学化学化工学院,江苏徐州,221116 |
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| 摘 要： | 目的:分析市售川芎饮片挥发油的化学成分。方法:用水蒸汽蒸馏法提取挥发油后,采用气相色谱-质谱法(GC-MS)分析。结果:1～5号样品挥发油中共鉴定出30种化学成分,主要成分为对-伞形花素(3.619%～9.528%)、4-松油醇(4.735%～8.474%)、β-芹子烯(4.516%～9.418%)、正丁烯基苯酞(4.270%～8.796%)、愈创木醇(2.743%～8.313%)、白菖烯(19.121%～41.659%)等。结论:市售川芎饮片的质量存在不同程度的差异。
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| 关 键 词： | 川芎饮片 挥发油 化学成分 气相色谱-质谱法 |
Analysis on Chemical Components of the Essential Oils of Processed Chuanxiong Rhizoma by GC-MS |
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| Cui Lijun,Zhang Guizhi,Wu Haiyan.Analysis on Chemical Components of the Essential Oils of Processed Chuanxiong Rhizoma by GC-MS[J].Asia-Pacific Traditional Medicine,2011,7(12):20-22. |
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| Authors: | Cui Lijun Zhang Guizhi Wu Haiyan |
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| Institution: | 1.School of Chemical and Chemical Engineering,Xu zhou Normal University,Jiangsu Xu zhou 221116; 2.Xuzhou Hospital of Traditional Chinese Medecine Jiangsu Xu zhou 221009,China) |
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| Abstract: | Objective：To analyse the chemical constituents of the essential oils of Processed Chuanxiong Rhizoma in different pharmacies.Methods：The essential oils were extracted by steam distillation from 5 batches of samples.Chemical constituents of The essential oils were analysed by GC-MS.Results：Chemical constituents of 30 kinds were identified from each essential oils.The characteristic compounds were all P-Cymene（3.619%~9.528%）,4-Terineol（4.735%~8.474%）,β-selinene（4.516%~9.418%）,Butylidenephthalide（4.270%~8.796%）,O-methoxyphenol（2.743%~8.313%）,Calarene（19.121%~41.659%）.Conclusion：It has significant difference compared with the quality of Anisi Stellati Fructus in different pharmacies. |
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| Keywords: | Processed Chuanxiong Rhizoma Volatile Oil Chemical Composition GC-MS |
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