| 小儿和胃利脾颗粒质量标准研究 |
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| 引用本文： | 邹禹,李卿,秦剑.小儿和胃利脾颗粒质量标准研究[J].中成药,2011,33(5):827-831. |
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| 作者姓名： | 邹禹 李卿 秦剑 |
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| 作者单位： | 1. 重庆市第九人民医院,重庆,400700
2. 重庆市中药研究院,重庆,400065 |
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| 摘 要： | 目的 建立小儿和胃利脾颗粒(鸡内金,山药,三七,黄芪等)质量标准.方法 采用薄层色谱法对小儿和胃利脾颗粒中三七、黄芪进行定性鉴别;采用高效液相色谱法测定小儿和胃利脾颗粒中三七皂苷R1、人参皂苷Rb1、人参皂苷Rg1、黄芪甲苷,色谱柱为C18柱,乙腈-水为流动相,检测器分别为紫外检测器、蒸发光散射检测器.结果 薄层色谱鉴别方法专属性强,斑点清晰,且阴性无干扰;三七皂苷R1、人参皂苷Rb1、人参皂苷Rg1、黄芪甲苷线性范围分别为0.42～4.20μg,r=0.999 7;0.76～7.60μg,r=0.999 8;0.70～7.ooμg,r=0.999 7及1.52～7.60μg,r=0.999 9.结论 本质量标准方法结果准确、重复性好,可有效控制该制剂的质量.
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| 关 键 词： | 小儿和胃利脾颗粒 三七皂苷R1 人参皂苷Rb1 人参皂苷Rg1 黄芪甲苷 |
Quality Standard of Xiao'er Hewei Lipi Granules |
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| ZOU Yu
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LI Qing
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QIN Jian.Quality Standard of Xiao'er Hewei Lipi Granules[J].Chinese Traditional Patent Medicine,2011,33(5):827-831. |
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| Authors: | ZOU Yu LI Qing QIN Jian |
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| Institution: | ZOU Yu1,LI Qing2,QIN Jian2(1.Chongqing The Ninth People's Hospital,Chongqing 400700,China,2.Chonging Academy of Chinese Materia Medica,Chongqing 400065,China) |
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| Abstract: | AIM To establish the quality standard of Xiao'er Hewei Lipi Granules(Galligigerii endothelium corneum,Dioscoreae Rhizoma,Notoginseng Radix et Rhizoma,Astragali Radix,etc).METHODS Identifications of Notoginseng Radix et Rhizoma and Astragali Radix were carried out by TLC.HPLC methods were used for the determination of notoginsenoside R1 and ginsenoside Rb1,ginsenoside Rg1 and astragoloside IV in Xiao'er Hewei Lipi Granules.A C18 column was used with the mobile phase of acetonitrile-water,the detectors were U... |
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| Keywords: | Xiao'er Hewei Lipi Granules notoginsenoside R1 ginsenoside Rb1 ginsenoside Rg1 astragaloside IV |
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