| 消炎洗散质量标准研究 |
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| 引用本文： | 欧燕,李希,张嵩,冯建安,邹俊波,黄嫣.消炎洗散质量标准研究[J].中成药,2011,33(4):629-633. |
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| 作者姓名： | 欧燕 李希 张嵩 冯建安 邹俊波 黄嫣 |
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| 作者单位： | 1. 成都中医药大学,四川,成都,610075
2. 四川省中医药科学院中医研究所,四川,成都,610031 |
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| 基金项目： | 四川省省级科研院(所)科研业务费资助项目(2009-4-272) |
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| 摘 要： | 目的 建立消炎洗散(苦参,黄柏,蛇床子,等)的质量标准.方法 采用TLC法对处方中苦参、黄柏、蛇床子、紫草、冰片进行定性鉴别;并采用HPLC测定苦参中苦参碱、氧化苦参碱,以及黄柏中盐酸小檗碱.结果 薄层色谱均检出苦参、黄柏、蛇床子、紫草、冰片;苦参碱在0.2008～2.008μg内呈良好的线性关系,r=0.99921.氧化苦参碱在0.2084～2.084μg内呈良好的线性关系,r=0.99885;平均回收率为99.68%,RSD为1.408%.盐酸小檗碱在0.2048～1.024μg内呈良好的线性关系,r=0.99992;平均回收率为99.76%,RSD为2.660%.结论 该方法 简便易行,重复性好,可作为该制剂质量控制标准.
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| 关 键 词： | 消炎洗散 苦参碱、氧化苦参碱、盐酸小檗碱 TLC HPLC |
Quality standard of Xiaoyanxi Powder |
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| OU Yan
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LI Xi
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ZHANG Song
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FENG Jian-an
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ZOU Jun-bo
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HUANG Yan.Quality standard of Xiaoyanxi Powder[J].Chinese Traditional Patent Medicine,2011,33(4):629-633. |
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| Authors: | OU Yan LI Xi ZHANG Song FENG Jian-an ZOU Jun-bo HUANG Yan |
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| Institution: | OU Yan1,LI Xi2,ZHANG Song2,FENG Jian-an2,ZOU Jun-bo1,HUANG Yan1(1.Chengdu University of TCM,Chengdu 610075,China,2.Institute of TCM,Sichuan Provincial Academy of Traditional Chinese Medical Science,Chengdu 610031,China) |
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| Abstract: | AIM To establish a quality standard of Xiaoyanxi Powder(Sophorae Flavescentic Radix,Phellodendri Chinensis Cortex,Cnidii Fructus,etc.).METHODS Sophorae Flavescentis Radix,Phellodendri Chinensis Cortex,Cnidii Fructus,Arnebiae Radix,Borneolum Syntheticum were identified by TLC.Matrine and oxymatrine in Sophorae flavescentis Radix,and berberine in Phellodendri Chinensis Cortex were determined by HPLC.RESULTS Sophorae flavescentis Radix,Phellodendri Chinensis Cortex,Cnidii Fructus,Arnebiae Radix,Borneolum Synth... |
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| Keywords: | Xiaoyanxi Powder matrine oxymatrine berberine TLC HPLC |
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