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壮药土垅大白蚁菌圃多糖的分析研究
引用本文:苏青,黄瑞松,刘婧. 壮药土垅大白蚁菌圃多糖的分析研究[J]. 中成药, 2011, 33(3): 468-471
作者姓名:苏青  黄瑞松  刘婧
作者单位:广西壮族自治区民族医药研究院,广西,南宁,530001
基金项目:广西自然科学基金课题项目(桂科自0832085)
摘    要:目的:建立土垅大白蚁菌圃多糖的分析测试方法,并进行不同产地,不同采集时间样品测定.方法:采用薄层色谱法和苯酚-硫酸比色法.结果:18个土垅大白蚁菌圃多糖样品的水解产物,均检测到D-葡萄糖、D-半乳糖、D-木糖等单糖组分,其总多糖含量为14.34%-23.91%,回收率为99.98%,RSD为0.738%.结论:该方法简便、准确、可靠,可为评价该药材质量标准提供参考.

关 键 词:土垅大白蚁菌圃  多糖  TLC  苯酚-硫酸比色法

Polysaccharides from Macrotermes annandalei(Silvestri) in Guangxi Zhuang Autonomous Region
SU Qing , HUANG Rui-song , LIU Jing. Polysaccharides from Macrotermes annandalei(Silvestri) in Guangxi Zhuang Autonomous Region[J]. Chinese Traditional Patent Medicine, 2011, 33(3): 468-471
Authors:SU Qing    HUANG Rui-song    LIU Jing
Affiliation:SU Qing,HUANG Rui-song,LIU Jing(National Medical Research Institute of Guangxi Zhuang Autonomous Region,Nanning 530001,China)
Abstract:AIM:To establish qualitative and quantitative analytical method for determining polysaccharide from Macrotermes annandalei(Silvestri).Sampling from various picking time and habitats in Guangxi Zhuang Au-tonomous Region,in China.METHODS:TLC and phenol-sulfuric acid methods were used to qualitative and quantitative analysis of polysaccharides.RESULTS:Acid hydrolyzates of polysaccharides in eighteen samples were viewed as D-glucose,D-galactose,D-xylose and other monosaccharide chemical composition.The total po...
Keywords:Macrotermes annandalei(Silvestri)  polysaccharide  TLC  phenol-sulfuric acid method  
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