| 红毛七化学成分的研究 |
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| 引用本文： | 但飞君,蔡正军,田瑛,郭志勇,褚立军. 红毛七化学成分的研究[J]. 中成药, 2011, 33(6): 1011-1014 |
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| 作者姓名： | 但飞君 蔡正军 田瑛 郭志勇 褚立军 |
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| 作者单位： | 1. 三峡大学天然产物研究与利用湖北省重点实验室湖北宜昌443002
2. 军事医学科学院放射与辐射医学研究所北京100085 |
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| 基金项目： | 湖北省生物资源保护与利用重点实验室开放基金项目(2007005) |
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| 摘 要： | 目的 研究红毛七的化学成分.方法 红毛七乙醇提取得到的浸膏分别用石油醚、三氯甲烷、乙酸乙酯和正丁醇萃取,正丁醇萃取物经硅胶柱层析和Sephadex LH-20柱层析得到化合物1～4,乙酸乙酯萃取物经硅胶柱层析得到化合物5～7,利用波谱学技术和化学方法对所得化合物进行结构鉴定.结果 鉴定7个化合物为:刺囊酸-α-L-吡喃阿拉伯糖苷(1)、常春藤皂苷元-3-O-β-D-葡萄吡喃-(1→2)-α-L-阿拉伯吡喃糖苷(2)、常春藤皂苷元-3-O-α-L-阿拉伯吡喃糖苷(3)、葳严仙皂苷元-3-O-α-L-阿拉伯吡喃糖苷(4)、β-豆甾醇(5)、羽扇豆醇(6)、胆甾醇(7).结论 化合物5,6,7为首次从该植物中分离得到,化合物1为首次从本属植物分离得到.
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| 关 键 词： | 红毛七 小檗科 化学成分 |
Chemical constituents of Caulophyllum robustum Maxim |
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| DAN Fei-jun , CAI Zheng-jun , TIAN Ying , GUO Zhi-yong , CHU Li-jun. Chemical constituents of Caulophyllum robustum Maxim[J]. Chinese Traditional Patent Medicine, 2011, 33(6): 1011-1014 |
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| Authors: | DAN Fei-jun CAI Zheng-jun TIAN Ying GUO Zhi-yong CHU Li-jun |
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| Affiliation: | DAN Fei-jun1,CAI Zheng-jun1,TIAN Ying2,GUO Zhi-yong1,CHU Li-jun1(1.Hubei Provincial Key Laboratory of Natural Products Research and Development,Three Gorges University,Yichang 443003,China,2.Institute of Radiation Medicine,The Academy of Military Medical Science,Beijing 100850,China) |
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| Abstract: | AIM To study the chemical constituents of Caulophyllum robustum Maxim.METHODS Caulophyllum robustum Maxim was extracted by alcohol at reduced pressure,extract obtained was mixed with water and then extracted with petroether,ethylacetate,chloroform,n-butanol.Compounds 1-4 were isolated with silica gel and Sephadex LH-20 gel from the n-butanol extract part.Compounds 5-7 were isolated with silica gel from the ethyl acetate extract part.Their structures were elucidated by spectroscopic and chemical methods.RESU... |
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| Keywords: | Caulophyllum robustum Maxim Berberidaceae chemical constituent |
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