| HPLC测定橘红丸中柚皮苷的含量 |
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| 引用本文： | 朱勇,陈淑映,吴子超. HPLC测定橘红丸中柚皮苷的含量[J]. 现代中药研究与实践, 2003, 17(3): 51-52 |
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| 作者姓名： | 朱勇 陈淑映 吴子超 |
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| 作者单位： | 1. 广东省佛山市中医院,广东,佛山 528000
2. 广东省佛山市药品检验所,广东,佛山 528000 |
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| 摘 要： | 目的 建立橘红丸中柚皮苷的含量测定方法。方法 采用高效液相色谱法。色谱柱 :Hypersil C1 8(4 .6 mm× 2 0 0 mm,5 μm) ;检测波长 :2 83nm;流动相 :甲醇 -冰醋酸 -水 (4 0∶ 1∶ 5 9) ;流速 :1 m l/ min。结果 回归方程为 :Y=2 .6 335× 1 0 6 X+1 5 1 2 1 ,r=0 .999,回收率 97.0 3 ,RSD为 1 .91 %。结论 结果证明本方法简便易行 ,结果准确 ,重现性好 ,可用于橘红丸的质量控制
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| 关 键 词： | HPLC 橘红丸 柚皮苷 含量测定 |
| 文章编号： | 1004-2199(2003)-0051-02 |
| 修稿时间： | 2003-04-25 |
Detetmination of Naringoside in Juhong Pill by HPLC |
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| ZHU Yong ,CHEN Shu ying ,WU Zi chao. Detetmination of Naringoside in Juhong Pill by HPLC[J]. Research and Practice on Chinese Medicines, 2003, 17(3): 51-52 |
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| Authors: | ZHU Yong CHEN Shu ying WU Zi chao |
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| Affiliation: | ZHU Yong 1,CHEN Shu ying 1,WU Zi chao 2 |
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| Abstract: | Objective To establish the determination method for naringoside in Juhong Pill. Methods HPLC analysis was carried out with Hypersil C 18 column(4.6 mm×200 mm,5 μm),detection wavelength at 283 nm,methanol acetic acid glacial water(40∶1∶59) as a mobile phrase,flow rate at 1ml/min. Results Regression equation is Y=2.6335×10 6X+15121 and r=0.999.The average recovery was 97.03% and RSD was 1.91%. Conclusion This method is simple, reliable and can be used for the quality control of Juhong Pill. |
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| Keywords: | HPLC Juhong Pills naringoside determination |
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