| 醋狼毒（月腺大戟）HPLC指纹图谱 |
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| 引用本文： | 狄恒建,庄 果,李俊松. 醋狼毒（月腺大戟）HPLC指纹图谱[J]. 药学与临床研究, 2014, 22(1): 53-55 |
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| 作者姓名： | 狄恒建 庄 果 李俊松 |
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| 作者单位： | 狄恒建 (江苏省食品药品检验所,南京,210008)； 庄果 (南京中医药大学江苏省中药炮制重点实验室,南京,210029)； 李俊松 (南京中医药大学江苏省中药炮制重点实验室,南京,210029)； |
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| 基金项目： | 国家公益性行业专项基金项目(项目编号：200807039)南京中医药大学中药学一级学科开放课题(项目编号：2011ZYX2-011) |
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| 摘 要： | 采用HPLC法,色谱条件:Welchorm-C18柱(4.6 mm×250 mm,5μm),在检测波长226 nm,柱温25℃下,以乙腈(A%)-水(B%)为流动相,流速1 mL·min-1梯度洗脱,初步建立了醋狼毒(月腺大戟)HPLC指纹图谱,确定醋狼毒(月腺大戟)中有24个共有峰。该方法准确、可靠、稳定,可以用于醋狼毒(月腺大戟)饮片的质量控制。
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| 关 键 词： | 月腺大戟 指纹图谱 醋炙 |
| 收稿时间： | 2013-08-14 |
| 修稿时间： | 2013-08-22 |
HPLC Fingerprints of Vinegar-processed Euphorbiae ebracteolatae Radix |
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| DI Heng-jian,ZHUANG Guo and LI Jun-song. HPLC Fingerprints of Vinegar-processed Euphorbiae ebracteolatae Radix[J]. Pharmacertical and Clinical Research, 2014, 22(1): 53-55 |
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| Authors: | DI Heng-jian ZHUANG Guo LI Jun-song |
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| Affiliation: | 1 Jiangsu Institute For Food and Drug Control, 210008,Nanjing; 2 Nanjing University of Traditional Chinese Medicine, Jiangsu Key Laboratory of Chinese Medicine Processing, 210046, Nanjing) |
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| Abstract: | Chromatographic fingerprints for the quality control of vinegar-processed Euphorbiae ebracte-olatae Radix were established on a Welchorm-C18 （250 mm×4.6 mm, 5μm） column with mobile phase ofacetonitrile and water by gradient elution at the flow rate of 1 mL·min-1. The column temperature was at 25℃ and detection wavelength was set at 226 nm. There were 24 common peaks selected in the chro-matograms, and all the common peeks were separated effectively. The precision, repeatability, and stabilityof this method were satisfying and can be used to identify and evaluate the quality of vinegar-processed Euphorbiae ebracteolatae Radix. |
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| Keywords: | Euphorbiae ebracteolatae Radix Fingerprints Vinegar-processed |
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