| 大孔吸附树脂分离纯化湖北贝母总生物碱的研究 |
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| 引用本文： | 张鹏,李娟,张国欣,皮慧芳,张勇慧,阮汉利,吴继洲. 大孔吸附树脂分离纯化湖北贝母总生物碱的研究[J]. 中成药, 2007, 29(1): 51-54 |
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| 作者姓名： | 张鹏 李娟 张国欣 皮慧芳 张勇慧 阮汉利 吴继洲 |
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| 作者单位： | 1. 华中科技大学同济医学院药学院,湖北,武汉,430030
2. 华中科技大学同济医学院附属同济医院,湖北,武汉,430030 |
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| 基金项目： | 国家中医药管理局新药开发专项基金 |
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| 摘 要： | 目的:研究湖北贝母总生物碱的纯化方法。方法:采用50%乙醇提取,D101型大孔吸附树脂分离纯化的方法。结果:提取物中的湖北贝母总生物碱含量达到74%。结论:D101型大孔吸附树脂适合分离纯化湖北贝母总生物碱。
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| 关 键 词： | 湖北贝母 总生物碱 大孔吸附树脂 |
| 文章编号： | 1001-1528（2007）01-0051-03 |
| 修稿时间： | 2005-12-17 |
Separation and purification of total alkaloids form Fritillaria hupehensis Hsiao et K. C. Hsia. with macroporous adsorption resin |
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| ZHANG Peng,LI Juan,ZHANG Guo-xin,PI Hui-fang,ZHANG Yong-hui,RUAN Han-li,WU Ji-zhou. Separation and purification of total alkaloids form Fritillaria hupehensis Hsiao et K. C. Hsia. with macroporous adsorption resin[J]. Chinese Traditional Patent Medicine, 2007, 29(1): 51-54 |
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| Authors: | ZHANG Peng LI Juan ZHANG Guo-xin PI Hui-fang ZHANG Yong-hui RUAN Han-li WU Ji-zhou |
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| Affiliation: | 1. Faculty of Pharmaceutical Sciences, Tongji Medical College of Huazhong University of Science and Technology, Wuhan 430030, China ;2. Tongji Hospital,Tongji Medical College,Huazhong University of Seience and Technology, Wuhan 430030, China |
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| Abstract: | AIM: To study the separation and purification of the total alkaloids of Fritillaria hupehensis Hsiao et K.C.Hsia. METHODS: Fritillaria hupehensis Hsiao et K.C.Hsia was extracted by 50% EtOH and purified by D_(101) macroporous adsorption resin. RESULTS: The content of the total alkaloids in the extracts was 74%.(CONCLUSION:)D_(101) macroporous adsorption resin is greatly effective for the isolation and purification of the total alkaloids of Fritillaria hupehensis Hsiao et K.C.Hsia. |
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| Keywords: | Fritillaria hupehensis Hsiao et K.C.Hsia total alkaloids macroporous adsorption resin |
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