| 高效液相色谱法测定速效牛黄丸中胆红素的含量 |
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| 引用本文： | 杨准,薛东升,张保彦. 高效液相色谱法测定速效牛黄丸中胆红素的含量[J]. 沈阳药科大学学报, 1993, 0(2) |
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| 作者姓名： | 杨准 薛东升 张保彦 |
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| 作者单位： | 河北保定地区药品检验所(杨准，薛东升)，保定市金钟制药厂(张保彦) |
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| 摘 要： | 本文报道了高效液相色谱法测定速效牛黄丸中胆红素含量的方法。采用进口ODS(美国)色谱柱,氯仿-甲醇(9∶1)为流动相,在450nm波长处检测,线性范围0.02～0.08mg/ml,平均回收率为99.9%,精密度以CV表示为2.7%,方法简便,准确。
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| 关 键 词： | 胆红素 速效牛黄丸 人工牛黄 高效液相色谱法 |
QUANTITATIVE DETERMINATION OF BILIRUBIN FROM SUXIAO NIUHUANG PILLS BY HIGH PERFORMANCE LIQUID CHROMATOGRAPHY |
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| Yang Zhun Xue Dongsheng Baoding Prefectural Institute for Drug Control Zhang Baoyan Baoding Jingzhong Pharmaceutical Factory. QUANTITATIVE DETERMINATION OF BILIRUBIN FROM SUXIAO NIUHUANG PILLS BY HIGH PERFORMANCE LIQUID CHROMATOGRAPHY[J]. Journal of Shenyang Pharmaceutical University, 1993, 0(2) |
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| Authors: | Yang Zhun Xue Dongsheng Baoding Prefectural Institute for Drug Control Zhang Baoyan Baoding Jingzhong Pharmaceutical Factory |
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| Affiliation: | Yang Zhun Xue Dongsheng Baoding Prefectural Institute for Drug Control Zhang Baoyan Baoding Jingzhong Pharmaceutical Factory |
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| Abstract: | In this paper, a High Performance Liquid Chromatography method for the determination of Bilirubin from Suxiao Niubuang Pills using import ODS column (USA) is described. The mobile phase is chloroform-methanol (9∶1). The concentration of bilirubin is measured at λ 450nm. The content is linear in the concentration range of 0,02～0.08 mg/ml. The average recovery is 99.9%. The precision of this method rapresented by the coefficient of variation is 2.7%. The method is simple and accurate. |
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| Keywords: | Bilirubin Suxiao Mubuang Pills Artificial Ox Gallstone HPLC |
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