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复感康颗粒质量控制方法研究
引用本文:覃伟,赵春景. 复感康颗粒质量控制方法研究[J]. 中国药房, 2005, 16(16): 1255-1257
作者姓名:覃伟  赵春景
作者单位:重庆医科大学附属第二医院药剂科,重庆市,400010
摘    要:目的:建立复感康颗粒的质量控制方法。方法:采用薄层色谱法对复感康颗粒中黄芪、白术、陈皮进行定性鉴别;采用高效液相色谱-蒸发光散射检测器法测定复感康颗粒中黄芪甲苷的含量。结果:在薄层色谱中可鉴别出黄芪、白术、陈皮;黄芪甲苷进样量在1.306μg~13.060μg范围内线性关系良好(r=0.9997),平均加样回收率为97.62%(RSD=1.72%)。结论:本方法简便、准确、重现性好,可用于复感康颗粒的质量控制。

关 键 词:复感康颗粒  质量控制  薄层色谱法  高效液相色谱-蒸发光散射检测器法
文章编号:1001-0408(2005)16-1255-03
收稿时间:2004-10-14
修稿时间:2004-10-14

Study of Quality Control Method for Fugankang Granules
QIN Wei,ZHAO Chunjing. Study of Quality Control Method for Fugankang Granules[J]. China Pharmacy, 2005, 16(16): 1255-1257
Authors:QIN Wei  ZHAO Chunjing
Abstract:OBJECTIVE:To establish the quality control method for fugankang granules.METHODS:Radix Astragali,Atr actylodes Macrocephala,Pericarpium Citri Reticulatae in fugankang granules were identified by TLC and the content of astraˉgaloside in fugankang granules was determined by HPLC-ELSD method.RESULTS:Radix Astragali,Atractylodes Macroˉcephala,Pericarpium Citri Reticulatae could be identified by TLC;Astragaloside showed good linear relationship within the range of1.306μg~13.060μg(r=0.9997),the average recovery was 97.62%(RSD=1.72%).CONCLUSION:The method is simple,accurate and with good reproducibility,which can be used as quality control for fugankang granules.
Keywords:Fugankang granules  Quality control  TLC  HPLC-ELSD
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