| 复感康颗粒质量控制方法研究 |
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| 引用本文： | 覃伟,赵春景.复感康颗粒质量控制方法研究[J].中国药房,2005,16(16):1255-1257. |
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| 作者姓名： | 覃伟 赵春景 |
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| 作者单位： | 重庆医科大学附属第二医院药剂科,重庆市,400010 |
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| 摘 要： | 目的:建立复感康颗粒的质量控制方法。方法:采用薄层色谱法对复感康颗粒中黄芪、白术、陈皮进行定性鉴别;采用高效液相色谱-蒸发光散射检测器法测定复感康颗粒中黄芪甲苷的含量。结果:在薄层色谱中可鉴别出黄芪、白术、陈皮;黄芪甲苷进样量在1.306μg～13.060μg范围内线性关系良好(r=0.9997),平均加样回收率为97.62%(RSD=1.72%)。结论:本方法简便、准确、重现性好,可用于复感康颗粒的质量控制。
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| 关 键 词： | 复感康颗粒 质量控制 薄层色谱法 高效液相色谱-蒸发光散射检测器法 |
| 文章编号： | 1001-0408（2005）16-1255-03 |
| 收稿时间： | 2004-10-14 |
| 修稿时间： | 2004年10月14 |
Study of Quality Control Method for Fugankang Granules |
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| QIN Wei,ZHAO Chunjing.Study of Quality Control Method for Fugankang Granules[J].China Pharmacy,2005,16(16):1255-1257. |
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| Authors: | QIN Wei ZHAO Chunjing |
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| Abstract: | OBJECTIVE:To establish the quality control method for fugankang granules.METHODS:Radix Astragali,Atr actylodes Macrocephala,Pericarpium Citri Reticulatae in fugankang granules were identified by TLC and the content of astraˉgaloside in fugankang granules was determined by HPLC-ELSD method.RESULTS:Radix Astragali,Atractylodes Macroˉcephala,Pericarpium Citri Reticulatae could be identified by TLC;Astragaloside showed good linear relationship within the range of1.306μg～13.060μg(r=0.9997),the average recovery was 97.62%(RSD=1.72%).CONCLUSION:The method is simple,accurate and with good reproducibility,which can be used as quality control for fugankang granules. |
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| Keywords: | Fugankang granules Quality control TLC HPLC-ELSD |
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