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Bergenia ciliate–Mediated Mixed-Phase Synthesis and Characterization of Silver-Copper Oxide Nanocomposite for Environmental and Biological Applications
Authors:Fazal Ur Rehman  Rashid Mahmood  Manel Ben Ali  Amor Hedfi  Mohammed Almalki  Amine Mezni  Wajid Rehman  Sirajul Haq  Humma Afsar
Affiliation:1.Department of Chemistry, University of Azad Jammu and Kashmir, Muzffarabad 13100, Pakistan; (F.U.R.); (R.M.); (H.A.);2.Department of Biology, College of Sciences, Taif University, P.O. Box 11099, Taif 21944, Saudi Arabia; (M.B.A.); (A.H.); (M.A.);3.Department of Chemistry, College of Science, Taif University, P.O. Box 11099, Taif 21944, Saudi Arabia;4.Department of Chemistry, Hazara University, Mansehra 21300, Pakistan;
Abstract:Bergenia ciliate (B. ciliate) leaf extract was used as a reducing and stabilizing agent for the synthesis of silver-copper oxide nanocomposite (Ag-CuO NC). Scanning and transmission electron microscopies (SEM and TEM) were used to examine the structural morphology, and the average particle size was determined to be 47.65 nm. The phase confirmation and crystalline structure were examined through the X-ray diffraction (XRD) technique, where cubic and monoclinic geometries were assigned to Ag and CuO. The energy dispersive X-ray (EDX), Fourier transform infrared (FTIR) and ultra-violet and visible (UV-Visible) spectroscopies were operated to analyse the elemental composition, functional groups and light absorption phenomena of the Ag-CuO NC. Under the full light spectrum, the photodegradation of Rhodamine 6G was recorded, and 99.42 percent of the dye degraded in 80 min. The Agar well diffusion method was followed to perform antibacterial activity against selected pathogens, and the activity was found to increase with increasing concentration of Ag-CuO NC. The ABTS free radical scavenging activity suggests that the activity of Ag-CuO NC is higher than ascorbic acid.
Keywords:copper oxide   silver   ascorbic acid   antioxidant   application
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