苦楝子中三萜成分的研究 |
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引用本文: | 周鹏,周琦,陈磊.苦楝子中三萜成分的研究[J].黑龙江医药,2011,24(3):381-382. |
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作者姓名: | 周鹏 周琦 陈磊 |
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作者单位: | 黑龙江中医药大学 |
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摘 要: | 目的:对苦楝子的甲醇提取物中的三萜成分进行研究.方法:利用硅胶,常压RP-C18硅胶,葡聚糖凝胶 LH-20以及制备液相色谱分离纯化,通过1D-NMR,2D-NMR以及EI-MS波谱数据鉴定化合物结构.结果:从苦楝子的甲醇提取物中共分离得到4个三萜化合物经鉴定为:Meliasenin B (Ⅰ),Meliasenin ...
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关 键 词: | 苦楝子 成分研究 三萜 |
Study on Triterpenoids of the Seed of Melia Azedarach L. |
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Institution: | Zhou Peng,et al Heilongjiang University of TCM |
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Abstract: | Objective:To study the chemical constituents of Melia azedarach L.Methods:Silica,RP-18,Sephadex HL-20 gel column and prep HPLC was employed to isolate and purify the constituents.Structures of the chemical constituents were elucidated by MS and NMR.Results:Six constituents were isolated and identified as meliasenin B(Ⅰ),meliasenin G(Ⅱ),12β-hydroxykulactone(Ⅲ),methyl kulonate(Ⅳ).Conclusion:CompoundsⅠ,Ⅱ and Ⅲ were firstly separated from Melia azedarach L. |
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Keywords: | Melia azedarach L Chemical constituents Triterpenoids |
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