紫外分光光度法快速测定复方制霉素栓的含量 |
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引用本文: | 郑桂英.紫外分光光度法快速测定复方制霉素栓的含量[J].中国药品标准,2000,1(2):29-31. |
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作者姓名: | 郑桂英 |
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作者单位: | 湖南省药品检验所 410001 |
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摘 要: | 目的:采用紫外分光光度法对制霉素中活性组份的含量测定。方法:用乙醚萃取赋形剂,制霉素用DMF溶解,再用5%DMF溶液稀释。紫外检测波长306nm。结果:通过实验方法考察,样品浓度每毫升在21-76制霉素单位范围内呈良好的线性关系。回收率为98.89/5(n=6)。结论:方法简便,灵敏,准确,可作为该制剂的快速测定方法。
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关 键 词: | 紫外分光光度法 测定 复方制霉素栓 含量 |
RAPID ASSAY OF NYSFUNGIN SUPPOSITORIES BY UV SPECTROPHOTOMETRY |
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Authors: | Zheng Guying |
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Institution: | Hu Nan Institute for Drug Control, ChangSha 410001 |
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Abstract: | Objective: UV spectrophotometry can be applied to determination of active components in nysfungin.Method: Ethyl ether is used as extract ancillary agent.The nysfungin is solvated by DMF.then dilute it with 5%DMF solution.Detection wavelength of 306nm was specified.Results: A methodological survey pointed out there is a good linearity between 21 to 76 of nysfungin units perml.The corresponding average recovery is 98.8%(n=6).inclusion: The method was found to be simple,quick and accurate for determination of nysfungin in its suppositories. |
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Keywords: | nysfungin thin-layer chromatography UV |
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