| 青银注射液的薄层鉴别及紫外含量测定 |
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| 引用本文： | 何兵,冯文宇,田吉,邱华荣.青银注射液的薄层鉴别及紫外含量测定[J].时珍国医国药,2006,17(4):546-547. |
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| 作者姓名： | 何兵 冯文宇 田吉 邱华荣 |
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| 作者单位： | 泸州医学院药研所,四川,泸州,646000 |
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| 基金项目： | 国家“九五”科技攻关资助项目(No.96-901-05-020) |
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| 摘 要： | 目的建立青银注射液的质量控制标准。方法采用薄层色谱法对青银注射液中的金银花、青蒿油进行定性鉴别,并用紫外分光光度法测定了其有效成分绿原酸的含量。结果在薄层层析色谱中均能检出金银花、青蒿油;总绿原酸的平均含量为19.38 mg/m l。结论薄层色谱鉴别方法简便、快速,重现性好,专属性强;而分光光度法测定绿原酸的含量,稳定性,精密度,重现性和回收率均较好,可用于青银注射液生产过程中的质量控制。
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| 关 键 词： | 青银注射液 青蒿油 金银花 薄层鉴别 紫外分光光度法 含量测定 |
| 文章编号： | 1008-0805（2006）04-0546-02 |
| 收稿时间： | 2005-07-01 |
| 修稿时间： | 2006-01-26 |
TLC Identification and UV Content Determination of QingYin Injection |
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| HE Bing,FENG Wen-yu,TIAN Ji,QIU Hua-rong.TLC Identification and UV Content Determination of QingYin Injection[J].Lishizhen Medicine and Materia Medica Research,2006,17(4):546-547. |
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| Authors: | HE Bing FENG Wen-yu TIAN Ji QIU Hua-rong |
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| Institution: | Institute of Materia Medica of Luzhou Medical College, Luzhou 646000 ; China |
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| Abstract: | ObjectiveTo establish the quality control standards for QingYin Injection.MethodsFlos Lonicerae and Artemisia oil in QingYin Injection were identified by TLC,content of active component in QingYin Injection were determined by UV.ResultsFlos Lonicerae and Artemisia oil could be detected by TLC,and the average content of total chlorogenic acid was 19.38 mg/ml.ConclusionTLC is simple and celerity,reproducibility and specificity are good,UV used in content determination of chlorogenic acid is stabile,precise,reproducible,and this method can be used for quality control in producing QingYin Injection. |
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| Keywords: | QingYin Injection Artemisia oil Flos Lonicerae TLC UV Content determination |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
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