| 复方栀黄片及栀子中栀子苷的含量测定 |
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| 引用本文： | 于晓蕾,张善勇,窦希波. 复方栀黄片及栀子中栀子苷的含量测定[J]. 齐鲁药事, 2006, 25(8): 477-478 |
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| 作者姓名： | 于晓蕾 张善勇 窦希波 |
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| 作者单位： | 鲁南制药集团股份有限公司,临沂,276006 |
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| 摘 要： | 目的应用反相高效液相色谱法测定复方栀黄片及栀子中栀子苷的含量。方法色谱柱为Zorbax SB C18色谱柱(5μm,4.6mm×250mm),流动相为乙腈-水(12∶88),检测波长为238nm,流速为1.0ml.min-1。结果栀子苷在0.13~2.08μg范围内进样量与峰面积呈良好线性关系(r=0.9999);平均加样回收率为98.83%,RSD=1.35%(n=3)。结论本方法测定结果准确、灵敏、重现性好。
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| 关 键 词： | 高效液相色谱法 复方栀黄片 栀子 栀子苷 含量测定 |
| 文章编号： | 1672-7738(2006)08-0477-02 |
Determination of Geniposide in Fufang Zhihuang Tablets and Cape Jasmine Fruit |
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| YU Xiao-lei,ZHANG Shan-yong,DOU Xi-bo. Determination of Geniposide in Fufang Zhihuang Tablets and Cape Jasmine Fruit[J]. qilu pharmaceutical affairs, 2006, 25(8): 477-478 |
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| Authors: | YU Xiao-lei ZHANG Shan-yong DOU Xi-bo |
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| Abstract: | OBJECTIVE To develop a method for determination of geniposide in Fufang Zhihuang Tablets and Cape Jasmine Fruit.METHODS Zorbax SB C_(18) column was used and the mobile phase was acetonitrile and water(12∶88).The detection wavelength was at 238nm,the flow rate was 1.0ml·min~(-1).RESULTS There was a good linear relationship between the concentration of geniposide and absorption area value in the range of 0.13～2.08μg(r=0.9999),the average recovery was 98.83%,RSD=1.35%(n=3).CONCLUSION The method was repeatable,sensitive and accurate. |
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| Keywords: | HPLC Fufang Zhihuang Tablets Cape Jasmine Fruit geniposide determination |
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