| 广枣四香滴丸中挥发性成分的GC指纹图谱研究 |
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| 引用本文： | 张丹,王霆,王淑美,付利娇,梁生旺,申洪超.广枣四香滴丸中挥发性成分的GC指纹图谱研究[J].广东药学院学报,2009,25(3):253-255. |
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| 作者姓名： | 张丹 王霆 王淑美 付利娇 梁生旺 申洪超 |
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| 作者单位： | 1. 河南中医学院,药学系,河南,郑州,450008
2. 广东药学院,中药学院,广东,广州,510006 |
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| 摘 要： | 目的建立复方广枣四香滴丸的指纹图谱。方法采用气相色谱法：DB-WAX毛细管柱（30m×0．25mm，0．25μm），进样口温度：200℃，检测器温度：240℃，分流比10：1，流速3mL／min，用“中药色谱指纹图谱相似度评价系统（2004A）”进行相似度评价，并对各峰进行化学成分归属。结果方法有良好的重复性、精密度和稳定性，建立的广枣四香滴丸GC指纹图谱确定19个共有峰，相似度在0．98以上。结论建立的指纹图谱可为广枣四香滴丸的质量控制提供依据。
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| 关 键 词： | 广枣四香滴丸 气相色谱法 指纹图谱 质量控制 |
GC fingerprints of volatile components in Guangzaosixiang dripping pills |
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| ZHANG Dan,WANG Ting,WANG Shu-mei,FU Li-jiao,LIANG Sheng-wang,SHEN Hong-chao.GC fingerprints of volatile components in Guangzaosixiang dripping pills[J].Academic Journal of Guangdong College of Pharmacy,2009,25(3):253-255. |
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| Authors: | ZHANG Dan WANG Ting WANG Shu-mei FU Li-jiao LIANG Sheng-wang SHEN Hong-chao |
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| Institution: | ZHANG Dan1,WANG Ting1,WANG Shu-mei2,FU Li-jiao2,LIANG Sheng-wang2,SHEN Hong-chao2(1.Traditional Chinese Medicine University of Henan,Zhengzhou,Henan 450008,China,2.School of Traditional Chinese Medicine,Guangdong Pharmaceutical College,Guangzhou,Gunagdong 510006,China) |
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| Abstract: | Objective To establish GC fingerprints of the volatile oil in Guangzaosixiang dripping pills.Methods Essential oil was extracted from the pills and detected by GC chromatography.Mathematical statistics software was used to evaluate the similarities of the peaks.Results Nineteen peaks were identified and their similarities were more than 0.98.Conclution The fingerprints was reliable and can be used in the quality control of the volatile oil in Guangzaosixiang dripping pills. |
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| Keywords: | Guangzaosixiang dripping pills GC fingerprints quality control |
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