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HPLC法测定三七止血胶囊中没食子酸的含量
引用本文:杨毅生,王栋,徐冬平,王仕平. HPLC法测定三七止血胶囊中没食子酸的含量[J]. 中国药品标准, 2007, 8(2): 70-72
作者姓名:杨毅生  王栋  徐冬平  王仕平
作者单位:1. 江西省食品药品检验所,南昌,330046
2. 江西中医学院
3. 江西省宜春市食品药品检验所,宜春,336000
摘    要:目的:建立HPLC法测定三七止血胶囊中没食子酸含量的方法。方法:色谱柱为C18,以甲醇-0.05%磷酸溶液(15:85)为流动相,检测波长271nm。结果:平均回收率为99.3%,RSD为0.47%(n=5)。结论:该法简便、灵敏、准确,重现性好。

关 键 词:三七止血胶囊  没食子酸  高效液相色谱法
文章编号:1009-3656(2007)-2-70-3

Determination of Gallic Acid in Sanqi Zhixue Capsule by HPLC
Yang Yi-sheng,Wang Dong,Xu Dong-ping and Wang Shi-ping. Determination of Gallic Acid in Sanqi Zhixue Capsule by HPLC[J]. , 2007, 8(2): 70-72
Authors:Yang Yi-sheng  Wang Dong  Xu Dong-ping  Wang Shi-ping
Affiliation:1.Jiangxi Institute for Food and Drug Control, Nanchang 330046; 2. Jiangxi Provincial Chinese Medicine College; 3. Yichun Institute for Food and Drug Control of Jiangxi Province, Yichun 336000
Abstract:Objective:To establish an HPLC method for the determination of Gallic Acid in Sanqi Zhixue Capsule.Method:The HPLC method was developed for the determination of Gallic Acid in Sanqi Zhixue Capsule on C18 column,using methanol-0.05% phosphoric acid solution(15:85) as mobile phase;detective wavelength at 271nm.Result:The average recovery is 99.3%and the RSD is 0.47%(n=5).Conclusion:The method is simple,sensitive and accurate with good reproducibility.
Keywords:Sanqi Zhixue Capsule   Gallic Acid  HPLC
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