| 补心安泰片中丹参酮ⅡA的含量测定 |
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| 引用本文： | 刘振华,崔佳,吴芳. 补心安泰片中丹参酮ⅡA的含量测定[J]. 中国医院用药评价与分析, 2009, 0(9): 687-688 |
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| 作者姓名： | 刘振华 崔佳 吴芳 |
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| 作者单位： | 武警总医院药剂科,北京市100039 |
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| 摘 要： | 目的：建立补心安泰片中丹参酮Ⅱ。的含量测定方法。方法：Themao C18柱（250mm×4．6mm，5μm）；流动相：甲醇-水（75：25）；流速：1．0mL·min^-1；检测波长：270nm；柱温：30℃结果：线形范围0．0790～0．6323μg；回归方程为Y=265732x-128293，R=0．9995；平均回收率为97．6％，RSD为0．77％（n=6）。结论：此方法简便、快速、准确，可用于补心安泰片中丹参酮ⅡA的含量测定。
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| 关 键 词： | 补心安泰片 丹参酮II。 HPLC |
Determination of Tanshinone IIA in Buxin Antai Tablets by HPLC |
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| LIU Zhen-hua,CUI Jia,WU Fang. Determination of Tanshinone IIA in Buxin Antai Tablets by HPLC[J]. Evaluation and Analysis of Drug-Use in Hospital of China, 2009, 0(9): 687-688 |
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| Authors: | LIU Zhen-hua CUI Jia WU Fang |
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| Affiliation: | (Dept. of Pharmacy, Armed Polices General Hospital, Beijing 100039, China) |
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| Abstract: | OBJECTIVE ： To establish a method for determination of Tanshinone IIA in Buxin Antai tablets. MEHTODS ： The sample determination was performed on C18 column（250 mm × 4.6 ram, 5 μm）. The mobile phase consisted of methanol - water（75： 15）at a flow rate of 1.0 mL/min. The detective wavelength was set at 270 mn and the column temperature was kept at 30 ℃ . RESULTS： The linear range of Tanshinone IIA was 0. 079 0μg - 0. 632 3μg, and the regression equation y = 265 732x - 128 293（ R = 0.999 5）. The average recovery rate was 97.6% （ RSD = 0.77%, n = 6）. CONCLUSION： The method is accurate, rapid and accurate, and it is applicable for the determination of Tanshinone IIA in Buxin Antai tablets. |
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| Keywords: | Buxin Antai tablets Tanshinone IIA HPLC |
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