| HPLC法测定桃红前列康丸中山柰素的含量 |
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| 引用本文： | 王霜. HPLC法测定桃红前列康丸中山柰素的含量[J]. 中国医药指南, 2012, 10(10): 432-433 |
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| 作者姓名： | 王霜 |
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| 作者单位： | 商丘市第一人民医院,河南商丘,476000 |
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| 摘 要： | 目的建立HPLC法测定桃红前列康丸中山柰素含量的方法。方法采用Eclipse XDB-C18色谱柱,甲醇-0.4%磷酸溶液(52∶48)为流动相;流速1.0mL/min;检测波长367nm。结果山柰素在0.01924～0.1732μg范围内线性关系良好(r=0.9999),平均回收率为98.32%,RSD=1.41%(n=6)。结论本方法操作简便,专属性强,结果准确,可用于桃红前列康丸的质量控制。
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| 关 键 词： | 山柰素 高效液相色谱法 含量测定 |
HPLC Determination of Kaempferol in Taohongqianliekang Pill |
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| WANG Shuang. HPLC Determination of Kaempferol in Taohongqianliekang Pill[J]. Guide of China Medicine, 2012, 10(10): 432-433 |
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| Authors: | WANG Shuang |
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| Affiliation: | WANG Shuang(Shangqiu First People＇s Hospital,Shangqiushi 476000,China) |
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| Abstract: | Objective To establish a HPLC method to determination of kaempferol in taohongqianliekang pill.Method The chromatographic system consisted of C18 column,using methanol-0.4% phosphate solution（52：48） as mobile phase.The content was detected at a waveleng of 367 nm,the flow rate was 1.0mL/min.Results The kaempferol have a good tincar rolatim in the range of 0.01924～0.1732μg（r=0.9999）,the average recovery was 98.32% and RSD=1.41%（n=6）.Conclusion The established method is accuracy,sensitive and simple.It can be used for quality control of taohongqianliekang pill. |
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| Keywords: | Kaempferol HPLC Determination |
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