| 平安丸的质量标准研究 |
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| 引用本文： | 张应辉,蒋帆,吴雪.平安丸的质量标准研究[J].中国药房,2011(35):3323-3325. |
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| 作者姓名： | 张应辉 蒋帆 吴雪 |
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| 作者单位： | 解放军第181医院药剂科; |
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| 摘 要： | 目的:建立平安丸的质量标准。方法:采用薄层色谱(TLC)法对平安丸中的青皮、陈皮、枳实、肉豆蔻、木香、延胡索进行定性鉴别;采用高效液相色谱法测定处方中橙皮苷的含量。结果:TLC斑点清晰、分离度好;橙皮苷进样量在0.1～1.1μg(r=0.9999)范围内与峰面积积分值呈良好线性关系,平均回收率为99.48%,RSD=0.62%(n=6)。结论:所建标准可用于平安丸的质量控制。
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| 关 键 词： | 平安丸 薄层色谱法 高效液相色谱法 橙皮苷 质量标准 |
Quality Standard of Ping'an Pills |
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| ZHANG Ying-hui,JIANG Fan,WU Xue.Quality Standard of Ping'an Pills[J].China Pharmacy,2011(35):3323-3325. |
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| Authors: | ZHANG Ying-hui JIANG Fan WU Xue |
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| Institution: | ZHANG Ying-hui,JIANG Fan,WU Xue(Dept.of Pharmacy,No.181 Hospital of PLA,Guilin 541002,China) |
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| Abstract: | OBJECTIVE： To establish the quality standard of Ping＇an pills. METHODS：Citrus reticulata, C. reiculata, Aurantii Fructas Immature, Myristica fraquans,Aucklandia lappa, Corydelis yanhusuo were identified by TLC. The content of hesperidin ＇was determined by HPLC. RESULTS：TLC spot was clear and well-separated. The linear range of hesperidin was 0.1-1.1 μg （r=999 9） with average recovery of 99.48% （RSD=0.62% ,n=6）. CONCLUSION： Established standard is suitable for the quality control of Ping＇ an pills. |
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| Keywords: | Ping'an pills TLC HPLC Hesperidin Quality standard |
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