| 艾燃烧生成物组分固相微萃取气相色谱质谱法定性分析 |
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| 引用本文： | 靳然,赵百孝,于密密,傅欣彤,陈有根,郭洪祝. 艾燃烧生成物组分固相微萃取气相色谱质谱法定性分析[J]. 北京中医药大学学报, 2011, 0(9): 632-636 |
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| 作者姓名： | 靳然 赵百孝 于密密 傅欣彤 陈有根 郭洪祝 |
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| 作者单位： | 北京中医药大学 北京 100029;北京市药品检验所 |
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| 基金项目： | 国家重点基础研究发展计划(973计划)项目(No.2009CB522906) |
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| 摘 要： | 目的 深入研究艾灸效应机制,为艾灸安全性研究奠定基础.方法 采用固相微萃取-气相色谱-质谱联用( SPME-GC-MS)技术对蕲艾绒燃烧生成的烟气(即艾烟)进行定性分析.结果 共分离出61个峰,其中鉴定出26种成分,检出物质分3部分,0 ～ 10 min为有呋喃结构的物质,10～40 min基本为芳香族化合物,40...
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| 关 键 词： | 艾燃烧生成物 艾烟 苯酚 固相微萃取-气相色谱-质谱联用 |
Qualitative analysis on components of moxa combustion products by solid-phase microextraction-gas chromatography-mass spectrography |
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| JIN Ran,ZHAO Bai-xiao,YU Mi-mi,FU Xin-tong,CHEN You-gen,GUO Hong-zhu. Qualitative analysis on components of moxa combustion products by solid-phase microextraction-gas chromatography-mass spectrography[J]. Journal of Beijing University of Traditional Chinese Medicine, 2011, 0(9): 632-636 |
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| Authors: | JIN Ran ZHAO Bai-xiao YU Mi-mi FU Xin-tong CHEN You-gen GUO Hong-zhu |
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| Affiliation: | JIN Ran1,ZHAO Bai-xiao1,YU Mi-mi2,FU Xin-tong2,CHEN You-gen2,GUO Hong-zhu2(1 School of Chinese Pharmacy,Beijing University of Chinese Medicine,Beijing 100029,2 Beijing Institute for Drug Control) |
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| Abstract: | Objective To study deeply the effective mechanism of moxibustion,and lay a foundation for the research on safety of moxibustion.Methods The combination technique of solid-phase microextraction-gas chromatography-mass spectrography(SPME-GC-MS) was used to analyse qualitatively the moxa smoke produced after moxa combustion.Results There were totally 61 peaks separated,and among them 26 components were identified,which consisted of three parts: components with furan structure at 0-10 minutes,aromatic compounds... |
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| Keywords: | moxa combustion products moxa smoke phenol combination of solid-phase microextraction-gas chromatography-mass spectrography |
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