| 正交试验法优选三黄丸提取工艺 |
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| 引用本文： | 马燕,喇孝瑾,白素芬,吕建东,张晓鹏,韩刚,王虹玉,喇万英.正交试验法优选三黄丸提取工艺[J].中国实验方剂学杂志,2012,18(10):31-33. |
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| 作者姓名： | 马燕 喇孝瑾 白素芬 吕建东 张晓鹏 韩刚 王虹玉 喇万英 |
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| 作者单位： | 1. 开滦(集团)有限责任公司医院分院,河北唐山,063000
2. 河北联合大学,河北唐山,063000 |
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| 基金项目： | 科技部国际科技合作项目(2008DFA31050) |
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| 摘 要： | 目的:优选三黄丸的提取工艺.方法:以盐酸小檗碱含量为指标,高效液相色谱法测定提取液中盐酸小檗碱含量,采用正交试验设计优选三黄丸的提取工艺.结果:三黄丸的最佳提取工艺为6倍量水提取2次,每次1.5h.结论:该提取工艺稳定,安全,简便易行.
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| 关 键 词： | 三黄丸 正交试验 提取工艺 高效液相色谱法 盐酸小檗碱 |
| 收稿时间： | 2011/12/4 0:00:00 |
Optimization of Extraction Technology for Sanhuang Pill by Orthogonal Test |
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| MA Yan,LA Xiao-jin,BAI Su-fen,LV Jian-dong,ZHANG Xiao-peng,HAN Gang,WANG Hong-yu and LA Wan-ying.Optimization of Extraction Technology for Sanhuang Pill by Orthogonal Test[J].China Journal of Experimental Traditional Medical Formulae,2012,18(10):31-33. |
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| Authors: | MA Yan LA Xiao-jin BAI Su-fen LV Jian-dong ZHANG Xiao-peng HAN Gang WANG Hong-yu and LA Wan-ying |
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| Institution: | Branch of Hospital, Kailuan Group Co.Ltd, Tangshan 063000, China;Hebei United University, Tangshan 063000, China;Hebei United University, Tangshan 063000, China;Hebei United University, Tangshan 063000, China;Hebei United University, Tangshan 063000, China;Hebei United University, Tangshan 063000, China;Hebei United University, Tangshan 063000, China;Hebei United University, Tangshan 063000, China |
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| Abstract: | Objective: To optimize extraction technology of Sanhuang pill. Method: Orthogonal experiment was used to optimize extraction technology of Sanhuang pill with the content of berberine hydrochloride as index, the content of berberine hydrochloride was determined by HPLC. Result: Optimum extraction process of Sanhuang pill was:extracted 2 times with 6 times the amount of water,1.5 h each time. Conclusion: This optimized technology of Sanhuang pill was simple, stable and effective. |
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| Keywords: | Sanhuang pill orthogonal test extraction technology HPLC berberine hydrochloride |
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