| 盆炎清灌肠剂的质量标准研究 |
| |
| 引用本文： | 邓世凯,张永萍,丁丽仙.盆炎清灌肠剂的质量标准研究[J].微量元素与健康研究,2012,29(1):18-21. |
| |
| 作者姓名： | 邓世凯 张永萍 丁丽仙 |
| |
| 作者单位： | 贵阳中医学院,贵阳,550002 |
| |
| 基金项目： | 贵州省中药现代化科技产业研究开发专项资金 |
| |
| 摘 要： | 目的:建立盆炎清灌肠剂的质量控制标准。方法:采用薄层色谱法检测制剂中的丹参、三棱、红藤和乌药;用高效液相色谱法测定制剂中丹酚酸B的提取量。结果:定性鉴别分离度好,专属性好;丹酚酸B进样量为0.0422～0.2532 mg/ml范围内与峰面积呈良好的线性关系,y=8620485.78x-9724.5(r=0.9997,n=6),测得制剂中的丹酚酸B含量稳定。结论:所建立的方法稳定可靠,准确,专属性好,可用于制剂的质量控制。
|
| 关 键 词： | 盆炎清灌肠剂 质量标准 |
Extraction Technology Research of Pen Yan Qing Enemas |
| |
| DENG Shi-kai
,
ZHANG Yong-ping
,
DING Li-xian.Extraction Technology Research of Pen Yan Qing Enemas[J].Studies of Trace Elements and Health,2012,29(1):18-21. |
| |
| Authors: | DENG Shi-kai ZHANG Yong-ping DING Li-xian |
| |
| Institution: | (Guiyang Traditional Chinese medicine college,Guiyang 550002,China) |
| |
| Abstract: | Objective: TO built the standard of Pen YanQin enemas′quilty controling.Method :Adopting the TLC to test the Salvia miltiorrhiza Bunge、Sparganium stdoniferum Buch.-Ham.、Sargentodoxa Cuneata(Oliv.)Rehd.et Wils、Lindera aggregata(Sims)Kosterm in the preparation,then using the HPLC to test the extraction of Salvianolic Acid B.Result: Qualitative identification had good separation and specificity,and Sal B and the injection volume was within the range of 0.0422～0.2532 mg/ml peakarea showed a good linear relationship,y=8620485678x-9724.5(r=0.9997,n=6),Preparations measured concentration in the stability of Sal B.Conclusion: The method is reliable,accurate and specific and can be used to control the quality. |
| |
| Keywords: | Pen YanQin Enemas Quality Standards |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
