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| 苦皮藤根皮的化学成分 | |
| 引用本文： | 朱文丽,沈国鹏,张海艳,赵天增.苦皮藤根皮的化学成分[J].中国实验方剂学杂志,2011,17(14):117-122. |
| 作者姓名： | 朱文丽 沈国鹏 张海艳 赵天增 |
| 作者单位： | 1. 郑州大学化工与能源学院,郑州450001;河南省科学院天然产物重点实验室,郑州450002 2. 郑州大学化工与能源学院,郑州,450001 3. 河南省科学院天然产物重点实验室,郑州,450002 |
| 基金项目： | 河南省发改委产业化研发专项 |
| 摘 要： | 目的:研究苦皮藤根皮醇提物的化学成分。方法:采用硅胶柱色谱和高效液相分离纯化,通过NMR鉴定化合物的结构。结果:分离并鉴定了11个化合物,分别为celahin B(1),celastrine A(2),celahin D(3),苦皮素E(4),苦皮素A(5),celangulatin C(6),苦皮藤素XIX(7),苦皮素P(8),苦皮素H(9),苦皮藤素III(10),苦皮素J(11)。结论:化合物1～3为首次从苦皮藤中分离得到。 |
| 关 键 词： | 苦皮藤 醇提物 化学成分 分离鉴定 |
| 收稿时间： | 2011/2/11 0:00:00 |
Chemical Constituents of Root Barks of Celastrus angulatus |
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| ZHU Wen-li,SHEN Guo-peng,ZHANG Hai-yan and ZHAO Tian-zeng.Chemical Constituents of Root Barks of Celastrus angulatus[J].China Journal of Experimental Traditional Medical Formulae,2011,17(14):117-122. | |
| Authors: | ZHU Wen-li SHEN Guo-peng ZHANG Hai-yan and ZHAO Tian-zeng |
| Institution: | Department of Chemical and Energy Engineering, Zhengzhou University, Zhengzhou 450001, China; Key Laboratory of Natural Products, Henan Academy of Science, Zhengzhou 450002, China;Department of Chemical and Energy Engineering, Zhengzhou University, Zhengzhou 450001, China;Key Laboratory of Natural Products, Henan Academy of Science, Zhengzhou 450002, China;Key Laboratory of Natural Products, Henan Academy of Science, Zhengzhou 450002, China |
| Abstract: | Objective: To study the chemical constituents from the alcohol extract of root bark of Celastrus angulatus. Method: The compounds,whose structures were confirmed by NMR spectra,were separated and purified by silica gel and preparative HPLC. Result: The structures of eleven compounds were conformed,they were celahin B(1),celastrine A(2),celahin D(3),angulatin E(4),angulatin A(5),celangulatin C(6),celangulin XIX(7),angulatin P(8),angulatin H(9),celangulin III(10),and angulatin J(11). Conclusion: Compound 1-3 were first found in C.angulatus. |
| Keywords: | Celastrus angulatus alcohol extract chemical constituents isolation and identification |
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