| 抗菌消炎胶囊质量标准研究 |
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| 引用本文： | 高玉琼,张译文,刘建华,刘文炜,霍昕. 抗菌消炎胶囊质量标准研究[J]. 中国实验方剂学杂志, 2011, 17(14): 90-92 |
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| 作者姓名： | 高玉琼 张译文 刘建华 刘文炜 霍昕 |
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| 作者单位： | 1. 贵州省生物技术研究开发基地,贵阳,550002
2. 中南大学湘雅药学院,长沙,410013 |
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| 摘 要： | 目的:建立抗菌消炎胶囊质量标准。方法:采用薄层色谱法对处方中的百部、大黄进行定性鉴别;采用高效液相色谱法测定该制剂中黄芩苷含量。结果:TLC鉴别分离度好,阴性对照无干扰。黄芩苷与样品中其他组分分离效果较好,Y=43 887 599.5X-4 893.8,线性范围0.01～0.16 g.L-1(r=0.999 9),平均回收率为98.56%,RSD为1.01%(n=6)。结论:建立的质量标准,简便易行,可用于抗菌消炎胶囊的质量控制。
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| 关 键 词： | 抗菌消炎胶囊 百部 大黄 黄芩苷 薄层色谱法 高效液相色谱法 |
| 收稿时间： | 2011-02-23 |
Study on Quality Standard of Kangjun Xiaoyan Capsule |
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| GAO Yu-qiong,ZHANG Yi-wen,LIU Jian-hu,LIU Wen-wei and HUO Xin. Study on Quality Standard of Kangjun Xiaoyan Capsule[J]. China Journal of Experimental Traditional Medical Formulae, 2011, 17(14): 90-92 |
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| Authors: | GAO Yu-qiong ZHANG Yi-wen LIU Jian-hu LIU Wen-wei HUO Xin |
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| Affiliation: | Guizhou Institute of Biotechnology Research and Development, Guiyang 550002, China;Xiangya School of Medicine Central South University, Changsha 410013, China;Guizhou Institute of Biotechnology Research and Development, Guiyang 550002, China;Guizhou Institute of Biotechnology Research and Development, Guiyang 550002, China;Guizhou Institute of Biotechnology Research and Development, Guiyang 550002, China |
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| Abstract: | Objective: To establish the quality standard of Kangjun Xiaoyan Capsule. Method :The identification of Radix stemonae and Radix et rhizome rhei were carried out by TLC. The content of baicalin was determined by HPLC. Result : The TLC spots were clear and separated well without interference of negative sample. The calibration curve of baicalin was linear in the range of 0.01-0.16 g ·L-1, Y=43 887 599.5X-4 893.8 (r=0.999 9). The average recovery was 98.56% with RSD 1.01% (n=6). Condusion : The method is simple, rapid and accurate. It can be used for the quality control of Kangjun Xiaoyan Capsule. |
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| Keywords: | Kangjun Xiaoyan Capsule Radix stemonae Radix et rhizome rhei baicalin TLC HPLC |
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