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| HPLC测定生脉糖浆（党参方）中五味子醇甲的含量 | |
| 引用本文： | 周琳梅,魏丽萍,吴春敏.HPLC测定生脉糖浆（党参方）中五味子醇甲的含量[J].海峡药学,2009,21(4):49-50. |
| 作者姓名： | 周琳梅 魏丽萍 吴春敏 |
| 作者单位： | 1. 福建中医学院药学系,福州,350003 2. 福建中医学院药学系,福州,350003;福建省药品检验,福州,350001 3. 福建省药品检验,福州,350001 |
| 摘 要： | 目的建立高效液相色谱法测定生脉糖浆中五味子醇甲的含量。方法采用Phenomenex Prodigy ODS3柱（5μm，4．6mm×250mm）．以甲醇-水（65：35）为流动相，流速为1．0mL·min-1。检测波长为250nmo结果五味子醇甲在7．9936-199．8400μg·mL-1。范围内呈良好的线性关系（r=1．000）：平均回收率分别为97．46％（n=9）。结论此方法简便、灵敏、准确，可用于生脉糖浆中五味子醇甲的含量测定。 |
| 关 键 词： | 五味子醇甲 生脉糖浆 HPLC |
Determination of schisandrin in Shengmai syrup by HPLC |
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| ZHOU Lin-mei,WEI Li-ping,WU Chun-min.Determination of schisandrin in Shengmai syrup by HPLC[J].Strait Pharmaceutical Journal,2009,21(4):49-50. | |
| Authors: | ZHOU Lin-mei WEI Li-ping WU Chun-min |
| Institution: | ZHOU Lin-mei, WEI Li-ping, WU Chun-min (1.F an Coil e of Traditional Chinese Medicine, Fuzhou 350003, China;2. Fujian Institute for Drug Control, Fuzhou 350001, China) |
| Abstract: | OBJECTIVE To establish an HPLC method for the determination of schisandrin in Shengmai syrup. METHODS The analysis was achieved on a Phenomenex Prodigy ODS3 column（5μm, 4.6mm ×250mm） using a mobile phase of methanol-water（65 ： 35）.The flow rate was 1.0mL·in- 1, and the detection wavelength was 250nm.RESULTS The linear range of schisandrin was 7.9936- 199.8400μg·mL-l（r= 1.000）, and the average recovery of schisandrin was 97.46 %. CONCLUSION The method was simple, accurate and sensitive. It can be used for the measurement of schisandrin. |
| Keywords: | HPLC |
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