| 反相高效液相色谱法测定吴茱萸中吴茱萸碱和吴茱萸次碱含量 |
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| 引用本文： | 张小梅,梁旭明,杨荣平,励娜,王云红.反相高效液相色谱法测定吴茱萸中吴茱萸碱和吴茱萸次碱含量[J].中国药业,2011,20(9):29-30. |
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| 作者姓名： | 张小梅 梁旭明 杨荣平 励娜 王云红 |
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| 作者单位： | 重庆市中药研究院,重庆,400065 |
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| 基金项目： | 重庆市科技攻关人才项目 |
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| 摘 要： | 目的建立测定吴茱萸中吴茱萸碱及吴茱萸次碱含量的反相高效液相色谱法。方法采用Boston Symmetrix ODS-R C18色谱柱(250 mm×4.6 mm,5μm),流动相为乙腈-0.04%辛烷磺酸钠溶液(50∶50),流速为1 mL/min,检测波长为225 nm。结果该法准确可靠,重现性好。结论反相高效液相色谱法可以同时测定吴茱萸中吴茱萸碱及吴茱萸次碱的含量。
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| 关 键 词： | 反相高效液相色谱法 吴茱萸 吴茱萸碱 吴茱萸次碱 含量测定 |
Content Determination of Evodiamine and Rutaecarpine in Fructus Evodiae by RP-HPLC |
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| Zhang Xiaomei,Liang Xuming,Yang Rongping,Li Na,Wang Yunhong.Content Determination of Evodiamine and Rutaecarpine in Fructus Evodiae by RP-HPLC[J].China Pharmaceuticals,2011,20(9):29-30. |
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| Authors: | Zhang Xiaomei Liang Xuming Yang Rongping Li Na Wang Yunhong |
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| Institution: | Zhang Xiaomei,Liang Xuming,Yang Rongping,Li Na,Wang Yunhong(Chongqing Academy of Chinese Materia Medica,Chongqing,China 400065) |
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| Abstract: | Objective To determine the content of evodiamine and rutaecarpine in Fructus Evodiae by RP-HPLC.Methods The separation was performed on Boston Symmetrix ODS-R column with acetonitrile -0.04% octane sulfonic acid sodium.The flow rate was 1 mL/min and the detection wavelength was 225 nm.Results This method is convenient and reliable.Conclusion This method can be used to determine the content of evodiamine and rutaecarpine in the Fructus Evodiae. |
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| Keywords: | RP-HPLC Fructus Evodiae evodiamine rutaecarpine content determination |
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