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高效液相色谱法测定肝泰胶囊中五味子甲素的含量
引用本文:沙瑞国,袁海龙,肖小河,李仙义. 高效液相色谱法测定肝泰胶囊中五味子甲素的含量[J]. 时珍国医国药, 2001, 12(5): 398-399
作者姓名:沙瑞国  袁海龙  肖小河  李仙义
作者单位:1. 中国人民解放军第66481部队医院,
2. 中国人民解放军第302医院,
3. 中国人民解放军第222医院,
摘    要:目的:建立肝泰胶囊中的五味子甲素的含量测定方法。方法:采用反相高效液相色谱法进行分离测定。C18为固定相,甲醇-水(75:25)为流动相,检测波长250nm。结果:加样回收率为100.56%,RSD为1.02%(n=6);3批样品五味子甲素含量分别为0.12%,0.11%,0.11%。结论:此方法快速、简便,可作为该药质量控制方法。

关 键 词:高效液相色谱法 肝泰胶囊 五味子甲素 中药的含量
文章编号:1008-0805(2001)05-0398-01
修稿时间:2001-01-02

Determination ofDeoxyschizandrin in Gantai Capsule by HPLC
SHA Rui-guo,YUAN Hai-long,XIAO Xiao-he,LI Xian-Yi. Determination ofDeoxyschizandrin in Gantai Capsule by HPLC[J]. Lishizhen Medicine and Materia Medica Research, 2001, 12(5): 398-399
Authors:SHA Rui-guo  YUAN Hai-long  XIAO Xiao-he  LI Xian-Yi
Affiliation:SHA Rui guo 1,YUAN Hai long 2,LI Xian yi 3,XIAO Xiao he 2
Abstract:Objective:To establish a determination method for deoxyschizandrin in traditional Chinese drug Gantai capsule. Methods:HPLC was developed for the determination, with the conditions of C18 as regular phase, methanol-water (75∶25) as mobile phase and detection wavelength at 250 nm. Results:The mean recovery of 100.56% (RSD 1.02%) for deoxyschizandrin was obtained the contents of deoxyschizanolrin in three batches sample were 0.12%, 0.11%, 0.11% respectively. Conclusion:The method was quick, accurate, and can be used for quality control.
Keywords:HPLC  Gantai capsule  Deoxyschizandrin  
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