| 健脑丸质量控制研究 |
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| 引用本文： | 杨林伟,张丽娟,宋新波,刘长松,刘晓帆.健脑丸质量控制研究[J].辽宁中医学院学报,2013(5):52-54. |
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| 作者姓名： | 杨林伟 张丽娟 宋新波 刘长松 刘晓帆 |
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| 作者单位： | [1]天津中医药大学,天津300193 [2]天津中一制药有限公司,天津300193 [3]北京中医药大学,北京100102 |
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| 摘 要： | 目的：对健脑丸的质量控制标准进行研究。方法：采用薄层色谱法对健脑丸中丹参、天麻进行定性鉴别。采用高效液相色谱法测定肉苁蓉中的松果菊苷和毛蕊花糖苷的含量。结果：用薄层色谱法鉴定出天麻素和丹参酮ⅡA的存在。采用HPLC法测定了该丸剂中毛蕊花糖苷的含量,方法精密度、稳定性、重复性良好,平均回收率为：松果菊苷97%,毛蕊花糖苷102%,RSD值为：松果菊苷0.91%,毛蕊花糖苷1.86%。结论：该方法简便、准确、重复性好,能有效控制健脑丸的质量。
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| 关 键 词： | 健脑丸 质量控制 丹参酮ⅡA 天麻素 毛蕊花糖苷 松果菊苷 |
Study on Quality Control of Jiannao Pill |
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| YANG Linwei,ZHANG Lijuan,SONG Xinbo,LIU Changsong,LIU Xiaofan.Study on Quality Control of Jiannao Pill[J].Journal of Liaoning College of Traditional Chinese Medicine,2013(5):52-54. |
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| Authors: | YANG Linwei ZHANG Lijuan SONG Xinbo LIU Changsong LIU Xiaofan |
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| Institution: | 1.Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China; 2.Tianjin Zhongyi Pharmacy Limited Company, Tianjin 300193, China ; 3.Beijing University of Chinese Medicine, Beijing 100102, China ) |
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| Abstract: | Objective ： To study the quality control of Jiannao Pill. Methods ： Salvia Miltiorrhiza and Cistanche salsa of Jiannao Pill were identified by TLC. HPLC was used to do quantitative analysis. Results： The existence of tanshinone II A and gastrodine was confirmed by TLC ; HPLC was used to quantitatively analyze the content of Verbascoside. The precision, stability and repeatability of the methods were good. Conclusion ： While the method is simple, the result shows high precision and repeatability, and it can be used to control the quality of Jiannao Pill. |
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| Keywords: | Jiannao Pill quality control tanshinone II A gastrodine acteoside echinacoside |
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