| 原子吸收及原子荧光法测定鸦胆子油乳注射剂中5种重金属及有害元素的残留量 |
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| 引用本文： | 李秀贤,周海莉,王怡君.原子吸收及原子荧光法测定鸦胆子油乳注射剂中5种重金属及有害元素的残留量[J].辽宁中医学院学报,2013(4):57-58. |
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| 作者姓名： | 李秀贤 周海莉 王怡君 |
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| 作者单位： | [1]辽宁中医药大学附属第二医院,辽宁省中医药研究院,辽宁沈阳110034 [2]辽宁省食品药品检验所,辽宁沈阳110023 |
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| 摘 要： | 目的：建立鸦胆子油乳注射剂中重金属及有害元素（铅、镉、铜、砷、汞）的分析检测方法。方法：采用石墨炉原子吸收法测定铅、镉元素;火焰原子吸收法测定铜元素;采用原子荧光法测定砷、汞元素;利用标准曲线法测定样品中重金属元素含量。结果：重金属元素检测分析方法考察结果5种重金属元素相关系数为0.9978～0.9998,回收率为94.8%～103.4%。结论：该方法简便、准确,可较好的用于鸦胆子油乳注射剂中重金属及有害元素的测定。
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| 关 键 词： | 鸦胆子油乳注射剂 重金属及有害元素 原子吸收分光光度法 原子荧光法 |
Atomic Absorption and Atomic Fluorescence Method for Determination 5 Kinds of Heavy Metal and Harmful Elements Residues in Brucea Javanica Oil Injection |
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| LI Xiuxian,ZHOU Haili,WANG Yijun.Atomic Absorption and Atomic Fluorescence Method for Determination 5 Kinds of Heavy Metal and Harmful Elements Residues in Brucea Javanica Oil Injection[J].Journal of Liaoning College of Traditional Chinese Medicine,2013(4):57-58. |
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| Authors: | LI Xiuxian ZHOU Haili WANG Yijun |
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| Institution: | ( l.The Second Affiliated Hospital of Liaoning University of Traditional Chinese Medicine, Liaoning Academy of Traditional Chinese Medicine, Shenyang 110034, Liaoning, China; 2.Liaoning Institute for Food and Drug Control, Shenyang 110023, Liaoning, China ) |
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| Abstract: | Objective： To establish the determination methods of five kinds of heavy metals and harmful elements （ lead, cadmium, copper, arsenic and mercury ） in Brucea Javanica Oil Injection. Methods ： The graphite furnace atomic absorption was used for determinations of lead and cadmium, flame atomic absorption method for determining copper, atomic fluorescence spectrometry for determining arsenic and mercury. Results ： The coefficient correlation was 0.9978-0.9998 and the recovery rate was 94,8% to 103.4%. Conclusion： This method is simple, accurate and can be better used to determine heavy metals and harmful elements in Brucea Javanica Oil Injection. |
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| Keywords: | Brucea Javanica Oil Injection heavy metal and harmful elements atomic absorptionspectrophotometry atomic fluorescence |
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