| 药物的荧光检测探针——9--蒽酰氯的合成 |
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| 引用本文： | 胡文祥,恽榴红. 药物的荧光检测探针——9--蒽酰氯的合成[J]. 军事医学科学院院刊, 1991, 0(3) |
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| 作者姓名： | 胡文祥 恽榴红 |
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| 作者单位： | 军事医学科学院毒物药物研究所，军事医学科学院毒物药物研究所 |
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| 摘 要： | 本文严格控制无水无醇条件,并改变试剂和溶剂用量,用9-蒽羧酸与亚硫酰氯反应,合成并纯化了性质活泼的9-蒽酰氯,作为荧光探针,定量分析微量和超微量药物。
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| 关 键 词： | 9-蒽酰氯 9-蒽羧酸 荧光探针 |
SYNTHESIS OF ANTHRACENE-O-CARBONYL CHLORIDE, A FLUORESCENT PROBE FOR DRUGS |
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| Hu Wenxiang Yun Liuhong. SYNTHESIS OF ANTHRACENE-O-CARBONYL CHLORIDE, A FLUORESCENT PROBE FOR DRUGS[J]. Bulletin of the Academy of Military Medical Sciences, 1991, 0(3) |
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| Authors: | Hu Wenxiang Yun Liuhong |
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| Abstract: | Anthracene-9-carbonyl chloride, used as a fluorescent detection probe in pharmaceutical trace analysis, was synthesized in dry chloroform by the reaction between anthracence-9-car boxylic acid and thionyl chloride distilled from sulfur or triphenylphosphite. |
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| Keywords: | anthracene-9-carbonyl chloride anthracence-9-carboxylic acid fluorescent detection probe |
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