| 痔宁洗剂质量标准研究 |
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| 引用本文： | 王丽芬,叶玉华.痔宁洗剂质量标准研究[J].中医药导报,2012,18(11):80-82. |
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| 作者姓名： | 王丽芬 叶玉华 |
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| 作者单位： | 1. 邵阳市中西医结合医院,湖南邵阳,422001
2. 邵阳市药品检验所,湖南邵阳,422001 |
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| 摘 要： | 目的:建立痔宁洗剂的质量标准。方法:采用TLC法对方中苦参和黄柏进行定性鉴别;采用HPLC法测定黄柏中盐酸小檗碱的含量。结果:在薄层色谱图斑点清晰,阴性对照品无干扰;盐酸小檗碱在0.0609-1.5225μg范围内呈良好线性关系,r=0.99996(n=6);平均回收率为98.8%,RSD%=1.5%,结论:该方法简便可行,专属性强,灵敏度高,重现性好,可用于痔宁洗剂的质量控制。
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| 关 键 词： | 痔宁洗剂 盐酸小檗碱 薄层色谱法 高效液相色谱法 |
Quality Stsndard for Zhining Lotion |
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| WANG Li-fen
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YE Yu-hua.Quality Stsndard for Zhining Lotion[J].GUIDING JOURNAL OF TCM,2012,18(11):80-82. |
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| Authors: | WANG Li-fen YE Yu-hua |
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| Institution: | 2 (l.Shaoyang Chinese and Westenm Medicine Hospital, Shaoyang 422001, China; 2.Shaoyang, Institute for Drug Contral, Shaoyang 422001, China) |
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| Abstract: | Objective： To establish a method for quality control of Zhimng Lotion. Methods： l hc Radtx sophorae ftavescen- tis and Cortex phellodelulri chinensis were identified by TLC, and the content of Berberine hydrochloride was determined by HPLC. Results： The TLC spots developed were fairly clear, the linear range of Naringin was 0.0609-1.5225g, the average recovery was 98.8%, RSD%=l.5%. Conclusion： This method is simple, specific, sensitive and available for quality control in Zhining I,otion. |
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| Keywords: | Zhining Lotion Berberine hydrochloride TLC HPLC |
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