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电子背散射衍射分析中的伪对称性误标及其克服
引用本文:孟利,杨平,李志超,崔凤娥. 电子背散射衍射分析中的伪对称性误标及其克服[J]. 中国体视学与图像分析, 2007, 12(4): 282-285
作者姓名:孟利  杨平  李志超  崔凤娥
作者单位:北京科技大学材料科学与工程学院,北京,100083
摘    要:本文基于在实验过程中遇到的误标数据,考察EBSD测量过程中发生误标的原因。涉及的材料包括密排六方结构(镁合金)、体心立方结构(电工钢)金属。统计结果表明,密排六方结构中的误标点(块)主要以30°(0001)和30°(1 1 2 12)的取向关系出现;体心立方结构中的误标点(块)多是30°〈111〉的取向关系,而且误标点具有重合位置点阵(CSL)关系。误标具有明显的晶粒取向选择性。最后提出一些的减少误标的办法。

关 键 词:电子背散射衍射(EBSD)  伪对称性  误标  取向
文章编号:1007-1482(2007)04-0282-04
修稿时间:2007-08-23

Mis-indexing of pseudosymmetry in EBSD analyses and its elimination
MENG Li,YANG Ping,LI Zhichao,CUI Fenge. Mis-indexing of pseudosymmetry in EBSD analyses and its elimination[J]. Chinese Journal of Stereology and Image Analysis, 2007, 12(4): 282-285
Authors:MENG Li  YANG Ping  LI Zhichao  CUI Fenge
Affiliation:MENG Li, YANG Ping, LI Zhichao, CUI Fenge (Department of Materials, University of Science and Technology Beijing, Beijing 100083, China)
Abstract:The reason of mis-indexing during EBSD measurement was examined based on the mis-indexing data encountered in the experiments. The materials involve HCP metal of magnesium alloys and BCC metal of electric steel. Statistical results reveal that orientation relationships of 30°〈0001〉 and 30°〈1 1 2 12〉 appears mostly in HCP magnesium alloys. Otherwise, 30°〈111〉 is the most relationship in the BCC metal; furthermore the mis-indexing spots have CSL boundaries relative to matrix. Mis-indexing exhibits obviously orientation dependence. At the end of this article, several means of reduction mis-indexing are mentioned.
Keywords:EBSD  pseudosymmetry  mis-indexing  orientation
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