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毛冬青中木质素苷类化学成分的研究
引用本文:杨鑫,丁怡,张东明. 毛冬青中木质素苷类化学成分的研究[J]. 中国中药杂志, 2007, 32(13): 1303-1305
作者姓名:杨鑫  丁怡  张东明
作者单位:1. 哈尔滨工业大学,食品科学与工程学院,黑龙江,哈尔滨,150090
2. 中国医学科学院,中国协和医科大学,药物研究所,北京,100050
摘    要:目的:研究毛冬青的化学成分。方法:溶剂法和色谱法分离化合物,波谱法鉴定其结构。结果:分离得到6个木质素苷类化合物,其结构鉴定为(7S,8R)-dihydrodehydrodiconiferyl alcohol 4-O-β-D-glucopyranoside(1),(-)-olivil-4′-O-β-D-glucopyranoside(2),(7S,8R)dehydrodiconiferyl alcohol 4-O-β-D-glucopyranosid(3),(+)-cyclo-olivil 6-O-β-D-glucopyranoside(4),(+)-medioresinol di-O-β-D-glucopyranoside(5),(+)-pinoresinol-4,4′-O-bisglucopyranoside(6)。结论:以上化合物均为首次从该属植物中分离得到。

关 键 词:毛冬青  木质素苷
文章编号:1001-5302(2007)13-1303-03
收稿时间:2006-12-05
修稿时间:2006-12-05

Studies on lignin glycosides in root from Ilex pubescens
YANG Xin; DING Yi; ZHANG Dong-ming. Studies on lignin glycosides in root from Ilex pubescens[J]. China Journal of Chinese Materia Medica, 2007, 32(13): 1303-1305
Authors:YANG Xin   DING Yi   ZHANG Dong-ming
Affiliation:1. School of Food Science and Engineering, Harbin Institute of Technology, Harbin 150086, China; 2. Institute of Materia Medica, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050, China
Abstract:OBJECTIVE: To study chemical constituents from Ilex pubescens. METHOD: The constituents were isolated by chromatographic method and the structures were identified on the basis of spectral alanlysis. RESULT: Six lignin glycosides were identified as (7S, 8R) dihydrodehydrodiconiferyl alcohol 4-O-beta-D-glucopyranoside (1), (-)-olivil-4'-O-beta-D-glucopyranoside (2), (7S, 8R) dehydrodiconiferyl alcohol 4-O-beta-D-gluco-pyranosid (3), (+)-cyclo-olivil 6-O-p-D-glucopyranoside (4), (+)-medioresinol di-O-beta-D-glucopyranoside (5), (+)-pinoresinol-4, 4'-O-bisglucopyranoside (6). CONCLUSION: All of them were isolated from this plant for the first time.
Keywords:Ilex pubescens   lignin glycosides
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