| 肉蔻五味丸质量标准研究 |
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| 引用本文： | 王旭梅,庞玉华.肉蔻五味丸质量标准研究[J].中国药房,2008,19(30):2382-2384. |
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| 作者姓名： | 王旭梅 庞玉华 |
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| 作者单位： | 1. 内蒙古赤峰市医院药剂科,赤峰市,024000
2. 内蒙古赤峰天奇制药有限责任公司,赤峰市,024000 |
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| 摘 要： | 目的:建立肉蔻五味丸的质量标准。方法:采用薄层色谱(TLC)法对肉蔻五味丸中的肉豆蔻、广枣与荜茇进行定性鉴别;采用高效液相色谱法对广枣中没食子酸的含量进行测定。结果:肉豆蔻、广枣与荜茇的TLC斑点清晰。没食子酸进样量在5.01～25.05μg·mL-1范围内与峰面积积分值呈良好线性关系(r=0.999 9);平均加样回收率为99.0%,RSD=1.10%(n=6)。结论:所建标准可用于肉蔻五味丸的质量控制。
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| 关 键 词： | 肉蔻五味丸 质量标准 薄层色谱法 高效液相色谱法 |
Quality Standard of Roukou Wuwei Pills |
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| WANG Xu-mei,PANG Yu-hua.Quality Standard of Roukou Wuwei Pills[J].China Pharmacy,2008,19(30):2382-2384. |
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| Authors: | WANG Xu-mei PANG Yu-hua |
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| Institution: | WANG Xu-mei,PANG Yu-hua(Dept.of Pharmacy, Inner Mongolia Chifeng Hospital,Chifeng 024000,China;Inner Mongolia Chifeng Tianqi Pharmaceutical Company Limited,Chifeng 024000,China) |
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| Abstract: | OBJECTIVE： To establish the quality standard of Roukou wuwei pills. METHODS： Myristica fragrans, Choerospondias axillaris and Piper longum in Roukou wuwei pills were identified qualitatively by TLC and the content of Gallic acid was determined by HPLC.RESULTS： Myristica, fragrans, Choerospondias axillaris and Piper longum showed clear TLC spots.Good linear relationship was achieved between Gallic acid and peak area when the concentration of Gallic acid was 5.01-25.05 μg·mL ^-1（ r = 0.999 9） .The average recovery rate was 99.0% （RSD = 1.10%, n = 6） .CONCLUSION： The established quality standard is suitable for the quality control of Roukou wuwei pills. |
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| Keywords: | Roukou wuwei pills Quality standard TLC HPLC |
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