| 大孔吸附树脂预分离后测定黄连及左金丸含量 |
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| 引用本文： | 刘映 李志忠. 大孔吸附树脂预分离后测定黄连及左金丸含量[J]. 中国药师, 2001, 4(2): 113-114 |
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| 作者姓名： | 刘映 李志忠 |
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| 作者单位： | 湖南古汉集团衡阳中药厂,衡阳市,421003 |
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| 摘 要： | 目的：探索大孔吸附树脂在中药材和中药制剂中分析生物碱类成分的方法。方法：对黄连及左金丸中化学成分用大孔吸附树脂D101进行预分离，反相高效液相色谱法测定其小檗碱的含量。结果：大孔吸附树脂D101在适当条件下对小檗碱具有较好的吸附和解吸附性能。结论：该方法分析中药材及其制剂中小檗碱含量时具有简便、快捷、排除杂质干扰等优点。
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| 关 键 词： | 大孔吸附树脂 反相高效液相色谱法 黄连 左金丸 小檗碱 中药 |
| 修稿时间： | 2000-06-09 |
Content Determination of Berberine in Rhizoma Coptidis and Zuojin Pills by Macroporous Adsorptive Resin-RP- HPLC |
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| Liu Ying,Li Zhizhong. Content Determination of Berberine in Rhizoma Coptidis and Zuojin Pills by Macroporous Adsorptive Resin-RP- HPLC[J]. China Pharmacist, 2001, 4(2): 113-114 |
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| Authors: | Liu Ying Li Zhizhong |
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| Abstract: | Objectives: To explore a proper method for the analyse of components in traditional Chinese medicinal materials and their preparations. Method: The berberine in Rhizoma coptidis and zuojing pill were pre-separated with macroporous ad.sorptive resin D101 , and the contents of berberine were determined by RP-HPLC. Result: Macroporous adsorptive resin had a better performance of adsorption and disadsorption in proper condition. Conclusion: This method is simpole , rapid, and interference of excluding impurities for determining the content of berberine in the traditional Chinese medicinal materials and their preparations. |
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| Keywords: | Resin macroporous adsorptive RP-HPLC Rhizoma coptidis Zuojin pill Berberine |
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