| 大蒜中蒜氨酸的分离与鉴定 |
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| 引用本文： | 常军民,孙万赋,张丽静,李新霞,陈坚. 大蒜中蒜氨酸的分离与鉴定[J]. 华西药学杂志, 2003, 18(6): 427-428 |
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| 作者姓名： | 常军民 孙万赋 张丽静 李新霞 陈坚 |
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| 作者单位： | 1. 新疆医科大学药学院,新疆,乌鲁木齐,830054
2. 新疆大学理化测试中心,新疆,乌鲁木齐,830046 |
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| 摘 要： | 目的 蒜氨酸的分离与鉴定。方法 采用硅胶色谱柱分离，物理、化学和光谱学方法鉴定结构。结果 确定了蒜氨酸的结构。结论 第一次利用1D-NMR和2D-NMR技术完整地确定了蒜氨酸中所有碳氢的信号归属。
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| 关 键 词： | 大蒜 蒜氨酸 分离 鉴定 中药 |
| 文章编号： | 1006-0103(2003)06-0427-02 |
| 修稿时间： | 2003-02-01 |
Identification and isolation of alliin in Allium sativum Linn |
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| CHANG Jun-min ,SUN Wan-fu ,ZHANG Li-jing ,LI Xin-xia ,CHEN Jian .College of Pharmacy,Xinjiang Medical University,Urumqi ,China,.Chemistry and Physics Detection Center,Xinjiang University,Urumqi ,China. Identification and isolation of alliin in Allium sativum Linn[J]. West China Journal of Pharmaceutical Sciences, 2003, 18(6): 427-428 |
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| Authors: | CHANG Jun-min SUN Wan-fu ZHANG Li-jing LI Xin-xia CHEN Jian .College of Pharmacy Xinjiang Medical University Urumqi China .Chemistry Physics Detection Center Xinjiang University Urumqi China |
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| Affiliation: | CHANG Jun-min 1,SUN Wan-fu 2,ZHANG Li-jing 2,LI Xin-xia 1,CHEN Jian 1 1.College of Pharmacy,Xinjiang Medical University,Urumqi 830054,China,2.Chemistry and Physics Detection Center,Xinjiang University,Urumqi 830046,China |
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| Abstract: | OBJECTIVE To identify and isolate alliin from Allium sativum.METHODS Allium was isolted by using bilicagel calumn chromato and was identified by chemical and spectroscopic evidence (IR,NMR).RESULTS Alliin structure was confirmed.CONCLUSION 13C and 1 H NMR signals of alliin were completely assigned by means of 1 H- 1 H COSY for the first time. |
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| Keywords: | Allium sativum Linn Alliin Isolation Identification |
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